VOC analysis results, sample AE12279, May 2002

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Data File : C:\HPCHEM\l\DATA\02MAY23\12287.D Vial: 11 Acq On : 24 May 2002 1:37 am Operator; 201-wb Sample : nys Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP051702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peale Number 1 3-Cyclobutene-l, 2-dione, 3,4-d Concentration Ranle 4

R.T. EstConc Area Relative to ISTD R.T. 15.78 0.03 ug/L 23511 1,4-DIFLUOROBENZENE 15.12 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 3-Cyclobutene-l,2-dione, 3,4-dihydr 114 C4H2O4 002892-51-5 4 2 3-Hexanone, 2-methyl- 114 C7H14O 007379-12-6 4 .3 2-Oxepanone 114 C6H10O2 000502-44-3 3 4 4-Heptanone 114 C7H14O' 000123-19-3 3 Abundance Scan 694 (15.784 min): 12287.D (-) m/z 114.15 100.00% 1 4

5000

63 RR \ ..... I, I....... 15.40 15.60 15.80 16.00 .............. y.).„i........ ”, m/z 62.95 29.10% Tl/Z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #2826: 3-Cyclobutene-1,2-dione, 3,4-dihydroxy- 29 58

5000 T T V 114 15.40 15.60 15.80 16.00 m/z 88.10 25.33% 86

10 17

20 ........ 30 40

40 68 ' I' '' ' I' ' '' I ' 50 60 70 80 90 A I ' ‘ 100 ‘ I 110 n" 120 Abundance #64192: 3-Hexanone, 2-methyl- 4)3 71

15.40 15.60 15.80 16.00 5000 m/z 56.85 23.63%

114

55 86 99 'I"" I'..... 'n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #64123: 2-Oxepanone 4)2 55 . 15.40 15.60 15.80 16.00 m/z 49.75 21.40%

552 27 84 70 114

' I ' ' ' ' I ' ' ' ' I ' tt/2-> 10 20 30 40 50 60 70 80 90 100 110 120 15.40 15.60 15.80 16.00

12287.D HP051702.M Tue May 28 09:16:08 2002 Page 1

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