Volatile organic compound analysis results, sample AE08016, April 2002

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Library Search Compound Report

Data File C:\HPCHEM\l\DATA\02apr05\8251F.D Vial: 12 Acg On 6 Apr 2002 3:11 am Operator: 201-wb Sample nyc fb Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP031802.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Cyclobutene-l ,2-dione, 3,4-d Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

15.73 0.04 ug/L 26719 1,4-DIFLUOROBENZENE 15.09

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Cyclobutene-l,2-dione, 3,4-dihydr 114 C4H2O4 002892-51-5 7 2 3-Hexanone, 2-methyl- 114 C7H14O 007379-12-6 4 3 2-Oxepanone 114 C6H10O2 000502-44-3 3 4 4-Heptanone 114 C7H14O 000123-19-3 3 Abundance Scan 691 (15.733 min): 8251 F.D (-) m/z 114.15 100.00% 1 4

8000

6000

4000 88 15.40 15.60 15.80 16.00 ^1° ^1^ , m/z 88.00 34.11% p--r-r-rp--r-r-rp--r-r-rpH-T-r-r--f--r-r-rpr-rVT-1-p-T-rp--r I ' ‘‘ I Tl/Z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #2826: 3-Cyclobutene-1,2-dione, 3,4-dihydroxy- 29 58

5000 114 15.40 15.60 15.80 16.00 m/z 63.15 24.92%

•n/z-> 10 17

20 30 40 40 50 60 70 80 90 68 86

100 110 120 M Abundance #64192: 3-Hexanone. 2-methyl- 43 71

15.40 15.60 15.80 16.00 lililil m/z 50.05 23.35% A 114

■n/z-> ' I ' ' ' ' I ' ' ' ' I ' 10 20 30 -Ji- 50 5.5 60 70 80 8690 99100 110 120 40 T-p-rS-r-f-T TTTiM-rT ' I ' ' ' ' I ' ' ' ' I ' ' T-rp-r

Abundance #64123: 2-Oxepanone 4l2 55 15.40 15.60 15.80 16.00 m/z 67.95 23.13%

5000

27 84 70 114

•n/z-> ' I ' ‘ 10 ' I ' ' ‘ ' I ' ‘ 20 30 ' I ' 40 50 60 70 80 X 100 110 120 15.40 15.60 15.80 16.00

8251F.D HP031802.M Sat Apr 06 03:54:48 2002 Page 1

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