VOC analysis results, sample AE12279, May 2002

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Library Search Compound Report

Data File C:\HPCHEM\l\DATA\02MAY23\12286F.D Vial 13 Acq On 24 May 2002 3:04 am Operator 201-wb Sample nys; fb Inst GC/MS Ins Mise Multiplr 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP051702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peale Number 3 Cyclotetrasiloxane, octamethyl Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 22.70 0.09 ug/L 84932 CHL0R0BENZENE-D5 21.78 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 78 2 Benzene, l-phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 9 3 3,6-Bis(N-dimethylamino)-9-ethylcar 281 C18H23N3 057103-04-5 9 4 6-A2aestra-l,3,5(10),6,8-pentaen-17 281 C18H19NO2 005144-20-7 5 Abundance Scan 1100 (22.696 min): 12286F.D (-) m/z 281.25 100.00% 2$1

5000

22.40 22.60 22.80 23.00 73 133 193 207 249 265 m/z 282.25 29.40% Ti/z-> 80 100 120 140 160 180 200 220 240 260 280 Abundance #41966: Cyclotetrasiloxane, octamethyl- 2B1

lililil 22.40 22.60 22.80 23.00 m/z 283.25 21.08% 73 133 207 I I j 163 177 ^^1^ ||... 235 m/z-> 80 100 120 140 160 180 200 220 240 260 280 Abundance #39643: Benzene, 1-phenyl-4-(2-cyano-2-phenylethenyl) 2$1

22.40 22.60 22.80 23.00 c [ililil m/z 133.05 12.93% A 253' 126 203 266 7 224 240 JI -n/z-> 80 100 120 140 X -p-n-r-t-r-rV- 160 180 200- 220 240 260 280 Abundance #39624: 3,6-Bis(N-dimethylamino)-9-ethylcarbazole 2 !1 22.40 22.60 22.80 23.00 m/z 265.20 10.59%

WiM 266

141 250 I 208 222 237 , •n/z--> 80 100 120 140 160 180 200 220 240 260 280 22.40 22.60 22.80 23.00

12286F.D HP051702.M Fri May 24 15:32:39 2002 Page 3

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