VOC analysis results, sample AE11905, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\02MAY22\T2156.D Vial: 9 Acq On : 23 May 2002 2:23 am Operator: 201-wb Sample : nyc Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP051702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peale Number 3 Cyclotetrasiloxane, octamethyl Concentration Rank 1 R.T. EstConc . Area Relative to ISTD R.T. 22.66 0.10 ug/L 68176 CHLOROBENZENE-D5 21.73 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 83 2 3,6-Bis(N-dimethylamino)-9-ethylcar 281 C18H23N3 057103-04-5 9 3 Benzene, l-phenyl-4-(2-cyan6-2-phen 281 C21H15N 027869-56-3 9 4 7a,9c-(Iminoethano)phenanthro[4,5-b 281 C18H19NO2 024695-70-3 9 Abundance Scan 1098 (22.662 min): 12156.D (-) m/z 281.25 100.00% 2$1

gSE

73 133 191 22.40 22.60 22.80 23.00 44 I I 249 265 jT-rT-i-p-i-TTp-rTTYrTT-ryiT^^ m/z 282.25 26.25% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260' 280 Abundance #41966: Cyclotetrasiloxane, octamethyl- 241

5000 22.40 22.60 22.80 23.00 m/z 283.25 19.22% 73 133 207 I 163177191 I 235249265 ryTnrT-i-q-rrVT-pHrTTqT-T-rTr-pT^^ -n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39624; 3,6-Bis(N-dimethylamino)-9-ethylcarbazole 2il1

22.40 22.60 22.80 23.00 552 m/z 133.15 12.05%

141 o-3c250 266 rt I 2082222^ I ■f- ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39643; Benzene, 1-phenyl-4-(2-cyano-2-phenylethenyl) .......... I, I,.,; 2$1 22.40 22.60 22.80 23.00 m/z 73.05 9.54% A 5000

„„„ 253 126 J I I X2242^WUI ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 22.40 22.60 22.80 23.00

12156.D HP051702.M Thu May 23 10:25:22 2002 Page 3

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