VOC analysis results, sample AE12279, May 2002

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Data File : C:\HPCHEM\l\DATA\02MAY23\12279.D vial: 4 Acq On : 23 May 2002 7:07 pm Operator: 201-wb Sample : nys ; Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP051702.M (RTE Integrator) Title : VOCs BY EPA.METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclotetrasiloxane, octamethyl Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 22.68 0.12 ug/L 85481 CHLOROBENZENE-D5 21.76 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 83 2 Benzene, l-phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 5 3 Morphinan, 7,8-didehydro-3-methoxy- 281 C19H23NO 001816-06-4 5 4 4-(1-Benzimidazyl)-7-nitro-2,1,3-ox 281 C13H7N5O3 091485-32-4 5 Abundance Scan 1099 (22.679 min): 12279.D (-) m/z 281.35 100.00% 2$1

5000

' I ' ‘ ' I ' ' ' ‘ I 73 133 191 207 249 22.40 22.60 22.80 23.00 44 I II I I m/z 282.35 31.69% -n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #41966: Cyclotetrasiloxane, octamethyl- 2$1

5000 "T 22.40 22.60 22.80 23.00 m/z 283.25 18.32% ... . ;.... J” ^^191 235249 265 -n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39643: Benzene, 1-phenyl-4-(2-cyano-2-phenylethenyl) 2$1

22.40 22.60 22.80 23.00 5000 m/z 133.05 11.68% h 253 126 203 I I I ' ' ' ' I'' ' m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39628: Morphinan, 7,8-didehydro-3-methoxy-17-methyl-6-meth 2$1 T 22.40 22.60 22.80 23.00 m/z 191.10 10.65%

552 44 160

'n/z-> l ■I ' ' 40 ' I'''' I' 60 80 I'''' I 188 >...... 100 120 140 160 180 200 220 240 260 280 226 266 I

22.40 22.60 22.80 23.00

12279.D HP051702.M Fri May 24 14:59:40 2002 Page 3

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