VOC analysis results, sample AE12531, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\02may24\12536.D Vial: 2 Acq On : 24 May 2002 11:08 pm Operator: 201-wb Sample : 524 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP051702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peale Number 3 Cyclotetrasiloxane, octamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

22.70 0.09 ug/L 94209 CHLOROBENZENE-D5 21.79

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 74 2 Benzene, l-phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 9 3 Morphinan, 7,8-didehydro-3-methoxy- 281 C19H23NO 001816-06-4 5 43,6-Bis(N-dimethylamino)-9-ethylcar 281 C18H23N3 057103-04-5 4 Abundance Scan 1100 (22.696 min); 12536.D (-) m/z 281.35 100.00% 2J 11

5000

73 ■p" ' 1 ' ' ' ' I ' ' ' ' I ' 133 191 22.40 22.60 22.80 23.00 45 I ,1.... ' ' I' ' ' ' I ' '' ‘ 1'''' I ... I ' ' ' ' m/z 282.35 31.92% ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #41966; Cycloletrasiloxane, octamethyl- 2!!1

Mig] 22.40 22.60 22.80 23.00 m/z 283.25 20.27% 73 ..... ( .'*.^^77.^.?'' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' I ' ' ' I ' ' ‘ ' I ' ' ' ' I 'n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39643; Benzene. 1-phenyl-4-{2-cyano-2-phenylethenyl) 2$1

22.40 22.60 22.80 23.00 5000 m/z 73.05 15.94%

253 126 fl I X^2242^^XAJ ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39628; Morphinan. 7.8-didehydro-3-methoxy-17-methyi-6-meth 2$1 22.40 22.60 22.80 23.00 m/z 133.05 13.19%

aaS 44 160

Tl/Z--> 1 40 60 80 100 120 140 160 180 200 220 240 260 280 188 226 266 I I'''' r 22.40 22.60 22.80 23.00

12536.D HP051702.M Fri May 24 23:48:10 2002 Page 3

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