VOC analysis results, sample AE11905, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\02MAY22\11905D.D Vial: 6 Acq On 22 May 2002 7:55 pm Operator: 201-wb Sample nyc; dup Inst : GC/MS Ins Mise Multiplr : 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP051702.M (RTE Integrator) Title : VOCs BY EPA METHOD.524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclotetrasiloxane, octamethyl Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

22.64. 0.10 ug/L 59700 CHLOROBENZENE-D5 21.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 83 2 Benzene, l-phenyl-4-(2-cyaho-2-phen 281 C21H15N 027869-56-3 9 3 Morphinan, 7,8-didehydro-3-methoxy- 281 C19H23NO 001816-06-4 5 4 4-(1-Benzimidazyl)-7-nitro-2,1,3-ox 281 C13H7N5O3 091485-32-4 5 Abundance Scan 1096 (22.643 min): 11905D.D (-) m/z 281.25 100.00% 2H1

5000

249 265 I 22.40 22.60 22.80 23.00 73 133 191 ' I'' 'I ■p-n-rp-rt-r m/z 282.25 32.35% ‘' I ‘' I' Tl/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #41966: Cyclotetrasiloxane, octamethyl- 2$1

lilHil 22.40 22.60 22.80 23.00 m/z 283.25 22.22% 73 133 163177^??^^ 235249 265 I rprT-TryT-rAH-yTTTTq-TT-TTyT-T^^ nn/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39643: Benzene, 1-phenyl-4-(2-cyano-2-phenylethenyl) 21 1

22.40 22.60 22.80 23.00 5000 m/z 73.05 13.43%

253 203 I 126 I J -n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39628: Morphinan, 7,8-didehydro-3-methoxy-17-methyl-6-meth 2$1 22.40 22.60 22,80 23.00 m/z 132.95 11.63%

5000

44 160 || 188 226 266 I I I'''' I'''' I'' I...... I'''' I''' ’ r T 1 m/2--> 40 60 80 100 120 140 160 180 200 220 240 260 280 22.40 22.60 22.80 23.00

11905D.D HP051702.M Thu May 23 09:22:27 2002 Page 2

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