VOC analysis results, sample AE12531, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\02may24\12536.D Vial: 2 Acq On : 24 May 2002 11:08 pm Operator: 201-wb Sample : 524 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\HP051702.M (RTE Integrator) Title VOCs BY EPA METHOD 524 Library C:\DATABASE\NBS75K.L ********************************************************************* Pea)< Number 2 Cyclotrisiloxane, hexamethyl- Concentration Ranlc 3

R.T. EstConc Area Relative to ISTD R.T.

17.96 0.05 ug/L 47099 1,4-DIFLUOROBENZENE 15.12

Hit# of 5 Tentative ID MW MolFoirm CAS# Qual

1 Cyclotrisiloxane, hexamethyl- 222 C6H18O3Si3 000541-05-9 74 2 Arsenous acid, tris(trimethylsilyl) 342 C9H27AsO3Si3 055429-29-3 64 3 N-Cyano-N',N',N'',N''-tetramethyl-1 207 C8H13N7 074150-88-2 9 4 2-Methyl-7-phenylindole 207 C15H13N 000000-00-0 9 Abundance Scan 822 (17.963 min): 12536.D (-) m/z 207.15 100.00% 207

5000

"T 96 133 191 17.60 17.80 18.00 18.20

Ti/z-> 44 . ..... I,, I " " I " ' • 11' " I A 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 m/z 208.15 21.27%

Abundance #70586: Cyclotrisiloxane, hexamethyl- 207

5000 17.60 17.80 18.00 18.20 m/z 96.20 14.52%

-n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #48300: Arsenous acid, tris(trimethylsilyl) ester . 207 I 17.60 17.80 18.00 18.20 5000 m/z 209.15 13.90% A

73 105 133 191 44 Il .1 I, 223239 327 ''' I'''' I'''' I'''' I TT-V-rp ' I'''' I'' tt/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #24502: N-Cyano-N’,N'.N",N"-tetramethyl-1,3.5-triazinetri ■T 207 17.60 17.80 18.00 18.20 m/z 191.10 12.66% 135 WHH 44 178 71 96 .4^ Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 17.60 17.80 18.00 18.20

12536.D HP051702.M Fri May 24 23:48:08 2002 Page 2

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