NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\l\DATA\02MAY23\12279D.D Vial; 4
Acq On ; 23 May 2002 7:51 pm Operator: 201-wb
Sample : nys; dup Inst : GC/MS Ins
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\HP051702.M (RTE Integrator)
Title : VOCs BY EPA METHOD 524
Library : C:\DATABASE\NBS75K.L
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Peak Number 2 Cyclotrisiloxane, hexamethyl- Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
17.95 0.05 ug/L 39163 1,4-DIFLUOROBENZENE 15.10
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclotrisiloxane, hexamethyl- 222 C6H18O3Si3 000541-05-9 74
2 Arsenous acid, tris(trimethylsilyl) 342 C9H27AsO3Si3 055429-29-3 64
3 N-Cyano-N',N',N'',N''-tetramethyl -1 207 C8H13N7 074150-88-2 9
4 N-(2-Acetylcyclopentylidene)cyclohe 207 C13H21NO 000000-00-0 9
Abundance Scan 820 (17.946 min): 12279D.D (-) m/z 207.15 100.00%
207
ilililil
96 133 17.60 17.80 18.00 18.20
44 I m/z 208.25 22.25%
Ti/z->
Ur I'''' I'''' I
40 60 80 100 120 140 160 180 200 220 240 260 280 300 320
Abundance #70586: Cyclotrisiloxane, hexamethyl-
207
SEW
17.60 17.80 18.00 18.20
m/z 209.05 13.61%
" I " ' ' I " " I " " I " " I ' ' ' N " ’' I I'''' I'
rn/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320
AbundanceI #48300; Arsenous acid, tris(trimethyisilyl) ester
207
I ‘ ' I ' ' I ' ' ' ' I ' ' ‘ ' I
17.60 17.80 18.00 18.20
5000 m/z 96.10 12.96%
73 105 133 191
44 h AUr-r
I''" I I" " I
223239
' I ‘' I'' p ''' I
327
Tn/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320
Abundance #24502; N-Cyano-N',N',N",N"-tetramethyl-1,3,5-triazinetri
207
17.60 17.80 18.00 18.20
m/z 133.05 12.65%
135
5000
44 178
71 96
I'''' I''' 'T'''' I
TT/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 17.60 17.80 18.00 18.20
12279D.D HP051702.M Fri May 24 15:01:10 2002 Page 2
NYC-WTC_000083612
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