VOC analysis results, sample AE12531, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\02may2 4\12531D.D Vial: 7 Acq On 24 May 2002 8:58 pm Operator: 201-wb Sample 524; dup. Inst : GC/MS Ins Mise Multiplr: 1,00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP051702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L

Peak Number 2 N-(2-Acetylcyclopentylidene)cy Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

17.96 0.09 ug/L 44666 1,4-DIFLUOROBENZENE 15.14

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-(2-Acetylcyclopentylidene)cyclohe 207 C13H21NO 000000-00-0 9 2 Hexahydropyridine, l-methyl-4- [4,5- 207 C12H17NO2 000000-00-0 9 3 N-Cyano-N',N',N'',N''-tetramethyl-1 207 C8H13N7 074150-88-2 9 4 Cyclotrisiloxane, hexamethyl- 222 C6H18O3Si3 000541-05-9 9 Abundance Scan 822 (17.962 min): 12531 D.D (-) m/z 207.15 100.00% 2(17

5000

‘n’ 17.60 17.80 18.00 18.20

~n/z-> 44 ' I ' ' ' ‘ I ' ' ' ' I ' 40 60 80 96

100 120 140 133

160 180 200 L m/z 208.25 21.88%

Abundance #24635: N-(2-Acetylcyclopentylidene)cyclohexylamine 2(1)7

164 124 TT-p-T SEB ' I ' ' ' ' 1 ' ' ' ' I ' 17.60 17.80 18.00 18.20 82 97 ^^0 150 m/z 209.25 15.31%

m/z--> 40 60 80 .IJII... L,|... 100 120 140 160 180 200 192

Abundance #24610: Hexahydropyridine, 1-methyl-4-[4,5-dihydroxyphenyl]- 207 70 42 17.60 17.80 18.00 18:20 97 5000 m/z 96.10 14.79% 82 136 ,| 150................... ^92 /A 123

Ti/z-> 40 60 80 100 120 140 160 180 200 Abundance #24502: N-Cyano-N'.N‘,N",N"-tetramethyl-1,3,5-triazinetri 2(1)7 ' I ' ' ' ' I ' 17,60 17.80 18.00 18.20 m/z 133.05 13.13% 135 5000 192 44 178 164 r-r-rX-^XX-r-T-r-rX 152 I, 71/z--> 40 60 80 100 120 140 160 180 200 17.60 17.80 18.00 18.20

12531D.D HP051702.M Fri May 24 21:38:30 2002 Page 2

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