VOC analysis results, sample AE12279, May 2002

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Data File : C:\HPCHEM\l\DATA\02MAY23\12284.D Vial: 8 Acq On : 24 May 2002 12:11 am Operator: 201-wb Sample : nys Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP051702.M {RTE Integrator) Title : VOCs BY EPA METHOD 524 Library- : C:\DATABASE\NBS75K.L ********************************************************************* Pea)< Number 3 Cyclotetrasiloxane, octamethyl Concentration Rank 1 R.T. . EstConc Area Relative to ISTD R.T. 22.70 0.10 ug/L 86332 CHLOROBENZENE-D5 21.76 ' Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 83 2 6,7-Benzo-phenothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0 9 3 3,6-Bis(N-dimethylamino)-9-ethylcar 281 C18H23N3 057103-04-5 9 4 Benzene, l-phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 9 Abundance Scan 1100 (22.696 min): 12284.D (-) m/z 281.25 100.00% 2$1

553

73 133 193 249 265 22.40 22.60 22.80 23.00 44 I ' ‘' I I I I I ' ‘ ' I ' ' ' m/z 282.35 30.08% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #41966: Cyclotetrasiloxane, octamethyl- 2$1

555] 22.40 22.60 22.80 23.00 m/z 283.25 16.58% 1631772?1L_ 235249265^ 73 133 I I ' I ' ' ' '' I ' ‘ ' I ‘ ' I ‘ ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39602: 6,7-Benzo-phenothia2ine-5.5-dioxide 2$1

22.40 22.60 22.80 23.00 5000 m/z 133.05 11.35%

217 I 232 102 118 T-p-T-TT-p- ' I ‘' ‘‘i ' m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39624; 3,6-Bis(N-dimethylamino)-9-ethylcarbazole 2$1 22.40 22.60 22.80 23.00 m/z 265.20 9.15% A 5000 266

141 208222236250 J. •n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 22.40 22.60 22.80 23.00

12284.D HP051702.M Eri May 24 15:07:18 2002 Page 3

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