VOC analysis results, sample AE11905, May 2002

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Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\02MAY22\12151F.D Vial: 12 Acq On : 23 May 2002 4:33 am Operator: 201-wb Sample : nyc; fb Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP051702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peale Number 2 Cyclotetrasiloxane, octamethyl Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

22.66 0.10 ug/L 57062 CHLOROBENZENE-D5 21.73

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 83 2 4-Amino-5-(4-acetylphenylazo)benzof 281 C14H11N5O2 000000-00-0 9 3 6,7-Benzo-phenothiazine-5 ,5-dioxide 281 C16H11NO2S 000000-00-0 9 4 6-Azaestra-l, 3,5(10),6,8-pentaen-17 281 C18H19NO2 005144-20-7 5 Abundance Scan 1097 (22.662 min): 12151F.D (-) m/z 281.35 100.00% 2$1

5000

T 22.40 22.60 22.80 23.00 73 133 191 m/z 282.35 26.06% n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #72646: Cyclotetrasiloxane, octamethyl- 2$1

5000 22.40 22.60 22.80 23.00 m/z 283.25 16.29% 73 265 133 . 177 193207 235 45 59 I '' ‘ I' ’ '' I I ' ''' I ' ''' I ' '' ' I '''' I -n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39574: 4-Amino-5-(4-acetylphenylazo)benzofurazan

liiiin 2$1

u. 22.40 22.60 22.80 23.00 m/z 191.10 10.09% 116 134 162 77

180194209 238252266 I " " I • ■ ■ I I'l,., I,,I, ■ I.,. ,'i,, I, I, Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 .260 280 Abundance #39602: 6,7-Benzo-phenothiazine-5,5-dioxide 2$1 22.40 22.60 22.80 23.00 m/z 73.05 9.51%

5000

217 I 332 _ 1?3ii8 189 , J ^1, 264 |

-n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 | 22.40 22.60 22.80 23.00

12151F.D HP051702.M Thu May 23 10:17:01 2002 Page 2

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