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VOC analysis results, sample AE03934, Feb 27 2002

Machine-extracted title · confidence 95%

Laboratory results for volatile organic compounds in sample AE03934 analyzed on February 27, 2002.

NYC-WTC_000020459–000020546

Folder label: “524 2/27/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\02FEB2 7\03941.D Vial: 19 Acq On : 27 Feb 2002 11:30 pm Operator: Sample : nyc Inst : 210 Mise : February 27, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP021102.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclotetrasiloxane, octamethyl Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

24.86 0.03 ug/L 14912 CHLOROBENZENE-D5 23.35

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclotetrasiloxane, octamethyl- 296 C8H2404Si4 000556-67-2 36 2 4-(2-Hydroxyethylamino) -l-oxo-2-phe 281 C16H15N3O2 000000-00-0 9 3 6,7-Benzo-phenothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0 5 4 3,6-Bis(N-dimethylamino)-9-ethylcar 281 C18H23N3 057103-04-5 5 Abundance scan 1892 (24.865 min): 03941. D (-) m/z 281.05 100.00% 281 8000

6000 4000 106 91 A A/ " A 207 249 2000 44 57 77 24.60 24.80 25.00 25.20 44 ,i I . I __________________ ।___I m/z 105.95 A 36.47% m/z-> 40 60'' 'sb' 100 120 140 160 180‘ 200 220‘ 240 260’ 280 Abundance #41966: Cyclotetrasiloxane, octamethyl- 281 8000 6000 4000 ' 24.60 24.80 25.00 25.20 m/z 281.95 30.27% 2000 73 133 tot 207 . per 1 m/z-> 40 I 60 1 80 ..........I.163 177.191 I.... . 249 225 . I 106’ 120 140 160 180 200 220 ‘240 260 280 Abundance #39604:4-(2-Hydroxyethylamino)-1-oxo-2-pheny-1,2-dihydrop 281 8000 237 250 24.60 24.80 25.00 25.20 6000 m/z 90.95 2 7.49% 4000 130 77 221 2000 102 174 194 niz-> 40 60 80 .III...... 160/2000/2060122301228 100 120 ‘ 140 + 1 260 262 ‘ | 280 ‘’ Abundance #39602: 6,7-Benzo-phenothiazine-5,5-dioxide 281 24.60 24.80 25.00 25.20 ' 8000 m/z 207.05 24.72% 6000 4000 I 217 2000 232 102 1 118 1 _ 189 204 1, 252264 ...r.............. , , m/z-> 40 ‘60 80 100 120 ‘ 140 160 180 200 220 240 260 280 24.60 24.80 25.00 25 20

03941.D HP021102.M Thu Feb 28 11:11:53 2002 Page 3

NYC-WTC_000020534

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NYC-WTC_000020534Source: NYC Law Department, mirrored locally

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