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VOC analysis results, sample AE12737, June 2002

Machine-extracted title · confidence 95%

Laboratory report for volatile organic compounds in sample AE12737 analyzed on June 3, 2002.

NYC-WTC_000083807–000083872

Folder label: “524 6/3/02

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Scanned page image, NYC-WTC_000083839
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Data File C:\HPCHEM\l\DATA\02june3\12734.D Vial: 3 Acq On 3 Jun 2002 5:52 pm Operator: 201-wb Sample 524 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP052902.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library- : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Benzoic acid, 4-[(trimethylsil Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 22.67 0.03 ug/L 29509 CHLOROBENZENE-D5 21.77 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Benzoic acid, 4-[(trimethylsilyl)am 281 C13H23NO2Si2 018406-05-8 5 2 6,7-Benzo-phenothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0 5 3 lH-Indole-3-carboxaldehyde, 2-(1,1- 281 C19H23NO 025584-28-5 5 4 Silanamine, N-[2,6-dimethyl-4-[(tri 281 C14H27NOSi2 072088-09-6 5 Abundance Scan 1098 (22.672 min): 12734.D (-) m/z 281.00 100.00% 21 11 8000

6000

ESB .... n. 22.40 22.60 22.80 23.00 m/z 282.00 30.53% -n/z->_______ 80 100 120 140 160 180 200 220 240 260 280 Abundance #72272: Benzoic acid, 4-[(trimethylsilyl)amino]-, trimethyl 2l i6 281

73 192 5000 222 . 22.40 22.60 22.80 23.00 m/z 283.00 21.69% 120 150207 " I' •n/2-> 80 100 120 140 160 180 200 220 240 260 280 Abundance #39602: 6,7-Ben2O-phenothiazine-5,5-dioxide 2$1

22.40 22.60 22.80 23.00 5000

217 232 I 102 118 189 204 i. ■n/z-> 80 100 120 140 160 180 200 220 240 260 280 Abundance #39632; 1 H-lndole-3-carboxaldehyde, 2-(1,1-dimethyl-2-prope 238 281 266

5000 169 201 225 252

'n/Z“> 80 100 120 140 160 180 200 220 240 260 280

12734.D HP052902.M Mon Jun 03 18:32:52 2002 Page 3

NYC-WTC_000083839

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NYC-WTC_000083839Source: NYC Law Department, mirrored locally

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