VOC analysis results, sample AE12737, June 2002

NYC 9/11 Public Portal Document Liicrary bearcn compouna xeporc

Data File C:\HPCHEM\l\DATA\02june3\12734.D Vial: 3 Acq On 3 Jun 2002 5:52 pm Operator: 201-wb Sample 524 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP052902.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library- : C:\DATABASE\NBS75K.L *******************************************************Tir*************

Peak Number 2 Pyrido[2,3-d]pyrimidine, 4-phe Concentration Rank 3 R.T. EstConc Area Relative toISTD R.T. 17.95 0.03 ug/L 25925 1,4-DIFLUOROBENZENE 15.11 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Pyrido[2,3-d]pyrimidine, 4-phenyl- 207 C13H9N3 028732-75-4 5 2 lH-Isoindole-1, 3{2H)-dione, 2-butyl 207 C12H17NO2 054934-85-9 5 3 4-Cyclohexene-l,2-dicarboximide, N- 207 C12H17NO2 028916-00-9 5 4 Acetamide, N-[4-(trimethylsilyl)phe 207 CllH17NOSi 017983-71-0 3 Abundance Scan 821 (17.953 mirV 12734.D (-) m/z 206.95 100.00% 207

5000

17.60 17.80 18.00 18.20 44 m/z 207.95 25.49% Ti/z-> 40 60 80 100 120 140 160 180 200 Abundance #24634: Pyrido[2,3-d]pyrimidine, 4-phenyl- 207

5000 179 17,60 17.80 18.00 18.20 77 m/z 43.85 5.19% , 103 152 126 -n/z-> 40 60 80 100 120 140 160 180 200 Abundance #24616: 1H-lsoindole-1,3(2H)-dione, 2-butyl-4,5,6.7-fetrahy 207 79 ■P 17.60 17.80 18.00 18.20 5000 165

111 124 136 ' I ' ' ' ' I ' ' I ' ' ’ ' I ' ' ' ' I ' ' ' I I ' ' •n/2-> 40 60 80 100 120 140 160 180 200 Abundance #24614: 4-Cyclohexene-1,2-dicarboximide, N-butyl-, cis- 2(1)7 80

5000 152 165

-n/z-> ' I ' ' ' ' I ' 40 60 136 ' I ' ' ' ' I ' ' ‘ ' I ' ' ' I ' ' 80 100 120 140 160 Tl^ 180 200 L

12734.D HP052902.M Mon Jun 03 18:32:49 2002 Page 2

NYC-WTC_000083838