VOC analysis results, sample AE12279, May 2002

NYC 9/11 Public Portal Document LiiDrary bearcn compouna Keporc

Data File : C:\HPCHEM\l\DATA\02MAY23\12282.D Vial: 6 Acq On : 23 May 2002 10:44 pm Operator: 201-wb Sample : nys Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method C:\HPCHEM\1\METHODS\HP051702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Pea]< Number 3 Cyclotetrasiloxane, octamethyl Concentration Ranlc 1

R.T. EstConc Area Relative to ISTD R.T.

22.68 0.09 ug/L 75597 CHL0R0BENZENE-D5 21.76

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 78 2 Benzene, l-phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 9 3 Morphinan, 7,8-didehydro-3-methoxy- 281 C19H23NO 001816-06-4 5 4 4-(1-Benzimidazyl)-7-nitro-2,1,3-ox 281 C13H7N5O3 091485-32-4 5 Abundance Scan 1099 (22.678 min): 12282.D (-) m/z 281.30 100.00% 2H1

552

22.40 22.60 22.80 23.00 45....... 73 133 193 249 265 I T-p-T-r-r-p--r-?-r-|- I'' “' 1 m/z 282.25 32.36% I '' ' ' I '' ‘ ' I ' ' ' ' I -n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #41966: Cyclotetrasiloxane, octamethyl- 2*1

5000 22.40 22.60 22.80 23.00 m/z 283.25 22.89% 133 207 73 ‘ I ' ' ' ' I J_ n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39643: Benzene, 1-phenyl-4-(2-cyano-2-phenylethenyl) 2$1

22.40 22.60 22.80 23.00 5000 m/z 133.05 13.07%

„„„ 253 126 203 I I y-rn-TT-p-TT-ry^VTTj-r-r-rTy •n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39628: Morphinan, 7,8-didehydro-3-methoxy-17-methyl-6-meth I ' ' ' ' I 2*1 22.40 22.60 22.80 23.00 m/z 73.05 12.67%

Saw 44 160

■n/z--> X 40 '' I'' '' I ‘ 60 ' I '' '' I ' 208 J 'I""I"' I 80 100 120 140 160 180 200 220 240 260 280 188 I 'I"I" 226 266

22.40 22.60 22.80 23.00

12282.D HP051702.M Fri May 24 15:04:20 2002 Page 3

NYC-WTC_000083634