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VOC analysis results, sample AE11905, May 2002

Machine-extracted title · confidence 95%

Laboratory report for volatile organic compounds in sample AE11905 analyzed on May 22, 2002.

NYC-WTC_000083395–000083562

Folder label: “524 5/22/02 - 5/23/02

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Scanned page image, NYC-WTC_000083442
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\02MAY22\11902.D Vial: 3 Acq On : 22 May 2002 5:45 pm Operator: 201-wb Sample : nyc Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP051702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peale Number 3 Cyclotetrasiloxane, octamethyl Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 22.65 0.12 ug/L 69512 CHLOROBENZENE-D5 21.73 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 83 2 6,7-Benzo-phenothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0 9 3 6-Azaestra-l,3,5(10),6,8-pentaen-17 281 C18H19NO2 005144-20-7 5 4 Morphinan, 7,8-didehydro-3-methoxy- 281 C19H23NO 001816-06-4 5 Abundance Scan 1096 (22.645 min); 11902.D (-) m/z 281.25 100.00% 2*1

5000

22.40 22.60 22.80 23.00 73 133 191 249 m/z 282.25 29.05% -n/z-> . 80 100 120 140 160 180 200 220 240 260 280 Abundance #41966: Cyclotetrasiloxane, octamethyl- 2$1

5000 22.40 22.60 22.80 23.00 m/z 283.25 17.59% 73 133 1Q1 207 I I ,235 249 265 | Tl/Z-> 80 100 120 140 160 180 200 220 240 260 280 Abundance #39602: 6,7-Benzo-phenothiazine-5,5-dioxide 2*1

22.40 22.60 22.80 23.00 5000 m/z 73.05 10.89%

217 232 . 102 118 ... ...... 189 204 ^ I 11 252264 II ■n/z-> 80 100 120 140 160 180 200 2201240260 280 Abundance #72282: 6-Azaestra-1,3,5(10),6,8-pentaen-17-one, 3-methoxy- 21 11 22.40 22.60 22.80 23.00 m/z.249.10 10.09%

225 5000 210 238 252 266 166 181 195 _ ■n/z--> 80 100 120 140 160 180I 200 220 240 260 280 22.40 22.60 22.80 23.00

11902.D HP051702.M Thu May 23 09:17:39 2002 Page 3

NYC-WTC_000083442

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NYC-WTC_000083442Source: NYC Law Department, mirrored locally

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