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VOC analysis results, sample AE12738, June 4 2002

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Laboratory report listing analytical results for volatile organic compounds in sample AE12738 analyzed on June 4, 2002.

NYC-WTC_000083874–000083923

Folder label: “524 6/4/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\l\DATA\02june04\12739F.D Vial: 10 Acq On 4 Jun 2002 7:49 pm Operator: 201-wb Sample nyc fb Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP052902.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Cyclotetrasiloxane, octamethyl Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 22.67 0.03 ug/L 34484 CHLOROBENZENE-D5 21.75 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 64 2 6,7-Benzo-phenothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0 9 3 14.alpha.-Morphinan, 7,8-didehydro- 281 C19H23NO 017939-34-3 5 4 6-Azaestra-l,3,5(10),6,8-pentaen-17 281 C18H19NO2 005144-20-7 5 Abundance Scan 1098 (22.674 min): 12739F.D (-) m/z 281.10 100.00% 21 1

5000

22.40 22.60 22.80 23.00 73 m/z 282.00 29.18% Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #72646: Cyclotetrasiloxane, octamethyl- 281

5000 22.40 22.60 22.80 23.00 m/z 283.10 18.00%

Wz-> 73 45 59 I 133 177 235 265 L 40 60 80 100 120 140 160 180 200 220 240 260 280 I Abundance #39602: 6,7-Benzo-phenothiazine-5,5-dioxide 2 !1 ...... ■^'"l I ' I I ' ' I ' ' 22.40 22.60 22.80 23.00 5000 m/z 72.95 16.15%

217 I 232 ft 102 118 264 I''''I''''I'' ‘I I ' ' '' I ' I'' '' I ■Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39631:14.alpha.-Morphinan, 7,8-didehydro-3-methoxy-17-niet 2$1 22.40 22.60 22 80 23 00 160

K 55m 44

116 188 226 266 I I I'''' I ■n/z-> 40 60 80 100 120 . 140 160 180 200 220 240 260 280

12739F.D HP052902.M Tue Jun 04 20:28:50 2002 Page 4

NYC-WTC_000083918

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NYC-WTC_000083918Source: NYC Law Department, mirrored locally

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