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VOC analysis results, sample AE11905, May 2002

Machine-extracted title · confidence 95%

Laboratory report for volatile organic compounds in sample AE11905 analyzed on May 22, 2002.

NYC-WTC_000083395–000083562

Folder label: “524 5/22/02 - 5/23/02

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Scanned page image, NYC-WTC_000083491
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\02MAY22\12151.D Vial: 5 Acq On : 22 May 2002 11:30 pm Operator: 201-wb Sample : nyc Inst : GC/MS Ins Mise : Multiplr: 1.0'0 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP051702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : .C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclotetrasiloxane, octamethyl Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

22.64 0.10 ug/L 70287 CHLOROBENZENE-D5 21.73

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 83 2 6,7-Benzo-phenothiazine-5 ,5-dioxide 281 C16H11NO2S 000000-00-0 9 3 6-Azaestra-l,3,5(10),6,8-pentaen-17 281 C18H19NO2 005144-20-7 5 4 Morphinan, 7,8-didehydro-3-methoxy- 281 C19H23NO 001816-06-4 5 Abundance Scan 1097 (22.645 min): 12151.D (-) m/z 281.25 100.00% 2*1

5000

' I ' ' ' ' I ' ' ' ' I 133 22.40 22.60 22.80 23.00 73 I 191 249 I m/z 282.25 29.24% Tl/Z-> 80 100 120 140 160 180) 200 220 240 260 280 Abundance #41966; Cyclotetrasiloxane, octamethyl- 2 1

5000 22.40 22.60 22.80 23.00 m/z 283.25 16.86% 73 133 207 I- 163 I I,., I 235 ^65^ m/z-> 80 100 120 140 160 180 200 220 240 260 280 Abundance #39602: 6,7-Benzo-phenothiazine-5,5-dioxide 2i 11 . .1 1 . 22.40 22.60 22.80 23.00 5000 m/z 133.05 14.72%

217 232 I 102 118 189 204 , |.| ,252264^ I ■n/z-> 80 100 120 140 160 180 200 220I 240 260 280 Abundance #72282: 6-Azaestra-1.3,5(10).6,8-pentaen-17-one, 3-methoxy- 2*1 22.40 22.60 22.80 23.00 m/z 73.05 11.68%

225 aSB 210 23g 252 266 166 181 195 Tl/Z--> 80 100 120 140 160 180 200 220 240 260 280 22.40 22.60 22.80 23.00

12151.D HP051702.M Thu May 23 10:15:31 2002 Page 3

NYC-WTC_000083491

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NYC-WTC_000083491Source: NYC Law Department, mirrored locally

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