VOC analysis results, sample AE12531, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\02may24\12532.D Vial: 4 Acq On : 24 May 2002 6:49 pm Operator: 201-wb Sample : 524 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP051702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peale Number 3 Cyclotetrasiloxane, octamethyl Concentration Rank 1

R.T. EstConc Area Relative to ISTD H-T.

22.73 0.06 ug/L 62690 CHL0R0BENZENE-D5 21.81

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 64 2 Benzene, l-phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 9 3 6,7-Benzo-phenothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0 5 4 14.alpha.-Morphinan, 7,8-didehydro- 281 C19H23NO 017939-34-3 5 Abundance Scan 1102 (22.729 min): 12532.D (-) m/z 281.30 100.00% 281

5000

73 133 191 249 265 22.40 22.60 22.80 23.00 44 I ' I'' ‘' I' I I I I'' ‘' I ‘' m/z 282.35 31.38% •n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #72646: Cyclotetrasiloxane, octamethyl- 281

T-r-p-T-r-ry 22.40 22.60 22.80 23.00 m/z 283.25 18.83% 265 I 73 133 177 \®32O7 235 45 59 I yrrTTy-r-r-rr-p-r-i^ I ’''' I'''' I'''' I'''' r L Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39643: Benzene, 1-phenyl-4-(2-cyano-2-phenylethenyl) 21 i1

22.40 22.60 22.80 23.00 m/z 191.10 12.59% 5000

253 126 203 I I •n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39602: 6,7-Benzo-phenothiazine-5,5-dioxide 281 22.40 22.60 22.80 23.00 m/z 133.05 11.80%

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102 118 ' I''' 'I' y.,i..J..|i... «<. Ti/z--> 40 60 80 100 120 140 160 180 200 220 240 260 280 22.40 22.60 22.80 23.00

12532.D HP051702.M Eri May 24 19:28:38 2002 Page 3

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