Volatile organic compound analysis results, sample AE07376, April 2002

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Data File C:\HPCHEM\l\DATA\02APR01\0401Bl.D Vial: 1 Acq On 1 Apr 2002 9:05 am Operator: 201-wb Sample lab blank Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: RTEINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP031802.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Pea)< Number 1 Cyclotetrasiloxane, octamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

22.70 0.11 ug/L 96797 CHLOROBENZENE-D5 21.78

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 64 2 6,7-Benzo-phenothiazine-5,5-dioxide. 281 C16H11NO2S 000000-00-0 9 3 l,2-Dihydroanthra[l,2-d]thiazole-2, 281 C15H7NO3S 000000-00-0 9 4 3,6-Bis(N-dimethylamino)-9-ethylcar 281 C18H23N3 057103-04-5 9 Abundance Scan 1100 (22.696 min): 0401 Bl.D (-) m/z 281.35 100.00% 2(!1

5000

73 191 22.40 22.60 22.80 23.00 45 I, 1 133 _L JlT 249 265 I__ L m/z 282.35 30.93% ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #41966: Cyclotetrasiloxane, octamethyl- 281

HlilM 22.40 22.60 22.80 23.00 m/z 73.05 18.40% 133 207 73 I I 235^y^ ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39602; 6,7-Benzo-phenothiazine-5.5-dioxide 2(!1

22.40 22.60 22.80 23.00 m/z 283.35 18.35% iBilil

217 232 102 118 I'''' I''' ’ I 189 I' '' ' 264 rp-n 1 'n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39586:1,2-Dihydroanthra[1,2-d]thiazole-2,6,11-trione 2i 1 22.40 22.60 22.80 23.00 m/z 191.10 16.90%

5000 209 253 76 127 153 170 225 I

-n/z-> ' I ' ' ' ' I ' ' ' I I '' 40 60 80 pVrp-r-r-iH-p-TY-r-f- 100 120 140 160 180 200 220 240 260 280 -X-rX 22.40 22.60 22.80 23.00

0401B1.D HP031802.M Eri Apr 05 12:26:06 2002 Page 1

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