VOC analysis results, sample AE11905, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\O2MAY22\119O1.D Vial 2 Acq On 22 May 2002 5:02 pm Operator 201-wb Sample nyc Inst GC/MS Ins Mise Multiplr 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP051702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************** Peale Number 3 Cyclotetrasiloxane, octamethyl Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

22.64 0.08 ug/L 53742 CHLOROBENZENE-D5 21.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 83 2 Benzene, l-phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 5 3 6,7-Benzo-phenothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0 3 4 1,2-Dihydroanthra[1,2-d]thiazole-2, 281 C15H7NO3S 000000-00-0 3 .bundance Scan 1097 (22.645 min): 11901.D (-) m/z 281.25 100.00% 2i 1

5000

73 133 207 22.40 22.60 22.80 23,00 44 I ' '' I ' p-r-r-p-T-T-^ry I I ''' ' I''' I ■p-r-n-p-m-j- m/z 282.25 33.33% •n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #72646: Cyclotetrasiloxane, octamethyl- 21 1

5000 22.40 22.60 22.80 23,00 m/z 283.25 20.63% 73 265 133 45 59 ! ' I'''' I' T' ''' I ' I ' ' ' ' I ' ' ‘ ' I '' ' ' I ' ' ' ' I L I '''' I -n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39643: Benzene, 1-phenyl-4-(2-cyano-2-phenylethenyl) .2*1

22.40 22.60 22.80 23.00 5000 m/z 133.05 11.57%

126 I I -p-T-rp-Th-T- I ' ' ' ' I JU242^djU 'n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39602: 6,7-Benzo-phenothiazine-5,5-dioxide 2B1 22.40 22.60 22.80 23.00 m/z 207.15 9.68%

5000-

217 I 232 102 118 264 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 22.40 22.60 22.80 23.00

11901.D HP051702.M Thu May 23 09:14:24 2002 Page 3

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