VOC analysis results, sample AE11905, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\02MAY22\12157.D Vial: 10 Acq On : 23 May 2002 3:06 am Operator: 201-wb Sample : nyc Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP051702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peale Number 2 Cyclotetrasiloxane, octamethyl Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 22.66 0.10 ug/L 70785 CHL0R0BENZENE-D5 21.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 83 2 6,7-Benzo-phenothiazine-5 ,5-dioxide 281 C16H11NO2S 000000-00-0 9 3 1,2-Dihydroanthra[1,2-d]thiazole-2, 281 C15H7NO3S 000000-00-0 5 4 3,6-Bis(N-dimethylamino)-9-ethylcar 281 C18H23N3 057103-04-5 5 Abundance Scan 1097 (22.661 min); 12157.D (-) m/z 281.25 100.00% 21(1

Wilil

44 73 I n-Tj-r . 133I ,. I'' '' I ' '' ' I '' 193 II 249 I '' ‘ I' ' ‘' I '''' I '' ' ‘ I ' " ■ 22.40 22.60 22.80 23.00 m/z 282.35 28.66% Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 )Kbundance #41966: Cyclotetrasiloxane, octamethyl- 2$1

5000 22.40 22.60 22.80 23.00 m/z 283.25 17.43% 73 133 207 I I 163177'’^,'' I 235249 265 rY’-TTrT‘yrT-VTyTVrryTT-TnjT-T^^ ■n/2-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39602: 6,7-Benzo-phenothia2ine-5,5-dioxide 2)11

22.40 22.60 22.80 23.00 ass m/z 133.15 12.04%

217

K 232 102118 I 264 I I'''' I''' ‘ I' ‘' I' ' I ' ’' ’ I ' •n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39586: 1,2-Dihydroanthra[1,2-d]thiazole-2,6,11 -trione 2$1 22.40 22.60 22.80 23.00 m/z 73.05 10.45% A 5000 209 253 76 127 153 170 I'' I ■ I. I •n/z--> 40 60 80 100 120 140 160 180 200 220 240 260 280 22.40 22.60 22.80 23.00

12157.D HP051702.M Thu May 23 10:27:02 2002 Page 2

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