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VOCs GC/MS analysis results, Jan 22-23 2002

Machine-extracted title · confidence 90%

Laboratory report showing volatile organic compound analysis results for sample AE01036 processed on January 22 and 23, 2002.

NYC-WTC_000003249–000003325

Folder label: “524 1/22/02”

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Scanned page image, NYC-WTC_000003298
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : .C:\HPCHEM\1\DATA\02JAN22\01036.D Vial: 14 Acq On : 22 Jan 2002 8:10 pm Operator: Sample : nyc Inst : 210 Misc : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP010802.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Cyclotetrasiloxane, octamethyl Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

26.64 0.03 ug/L 10397 CHLOROBENZENE-D5 25.16

Hit# of 5 Tentative ID MW MolForm CAS# Qual --------------------------------------------------------------------- 1 Cyclotetrasiloxane, octamethyl- 296 C8H2404Si4 000556-67-2 56 2 6,7-Benzo-phenothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0 5 3 1,2-Dihydroanthra[1,2-d]thiazole-2, 281 C15H7NO3S 000000-00-0 5 4 3.6-Bis(N-dimethvlami nn) -9-Pt hvl r'. r 2 1 C1 Au9'3N ,71 nr-n .-r, r, undance Scan 2034 (26.644 min): 01036.D (-) m/z 281.05 100.00% 21

5000 91 106 249 26.40 26.60 26.80 27.00 39 133 193 m z 91.05 31.91% z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 undance #72646: Cyclotetrasiloxane, octamethyl- 21

5000 26.40 26.60 26.80 27.00 m z 281.95 2i.990 73 265 45 59 133 177 193 207 235 z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 undance #39602: 6.7-Benzo-phenothiazine-5,5-dioxide 21

26.40 26.60 26.80 27.00 5000 m z 283.05 19.28%

217 232

i/z-> 40 60 102 118 80 100 120 140 160 180 200 220 240 189 204 J 252264 260 280 Abundance #39586:1,2-Dihydroanthra[1,2-d]thiazole-2,6,11-trione 2 1 26.40 26.60 26.80 27.00 m z 106.15 15.94%

5000

209 253 76 127 153 170 196 225 z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 26.40 26.60 26.80 27.00

01036.D HP010802.M Wed Jan 23 09:46:22 2002 Page 5

NYC-WTC 000003298

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NYC-WTC_000003298Source: NYC Law Department, mirrored locally

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