VOC analysis results, sample AE12531, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\l\DATA\02may24\12538.D Vial: 4 Acq On 25 May 2002 12:35 am Operator: 201-wb Sample 524 Inst : GC/MS Ins. Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP051702.M {RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peale Number 3 Cyclotetrasiioxane, octamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

22.71 0.08 ug/L 85893 CHLOROBENZ ENE-D5 21.78

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclotetrasiioxane, octamethyl- 296 C8H24O4Si4 000556-67-2 78 2 6,7-Benzo-phenothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0 9 3 1,2-Dihydroanthra [1,2-d]thiazole-2, 281 C15H7NO3S 000000-00-0 5 4 3,6-Bis(N-dimethylamino)-9-ethylcar 281 C18H23N3 057103-04-5 5 Abundance Scan 1101 (22.713 min): 12538.D (-) m/z 281.25 100.00% 2(11

5000

73 191 207 249 22.40 22.60 22.80 23.00 44 I _______ I I p--rT-r-p-T-iH-]-r-rT-rYT-r-r-q--r-r^^ I I m/z 282.35 28.49% •n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #72646: Cyclotetrasiioxane, octamethyl- 2$1

5000 —T-r-i-r-r-r-r-,-,

22.40 22.60 22.80 23'00 m/z 283.25 17.18%

Ti/z-> Abundance 73 45 59 I 133 177^93207 ' ' I ' ‘ ' I ' ' ' ' I ' 40 60 80 100 120 140 160 180 200 220 240 260 280 !'

#39602: 6,7-Benzo-phenothiazine-5,5-dioxide xJ 2$1

22.40 22.60 22.80 23.00 row m/z 133.05 12.62%

217 I 232 102 118 264 I ’ I' ’ ’ ’I' m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39586: 1,2-Dihydroanthra[1,2-d]thiazole-2.6,11-trione 2$1 22.40 22.60 22.80 23.00 m/z 73.05 12.30%

5000

209 A 253 76 127 153 170 I''‘'I'' '' I' ' I -n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 22.40 22.60 22.80 23.00

12538.D HP051702.M Sat May 25 01:14:50 2002 Page 3

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