VOC analysis results, sample AE12737, June 2002

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Data File C:\HPCHEM\l\DATA\02june3\12736.D Vial: 5 Acg On 3 Jun 2002 7:18 pm Operator: 201-wb Sample 524 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP052902.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library- : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 6,7-Benzo-phenothiazine-5,5-di Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 22.69 0.03 ug/L 28971 CHLOROBENZENE-D5 21.77 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 6,7-Benzo-phenothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0 5 2 1,2-Dihydroanthra [1,2-d]thiazole-2, 281 C15H7NO3S 000000-00-0 5 3 3,6-Bis(N-dimethylamino)-9-ethylcar 281 C18H23N3 057103-04-5 5 4 Benzene, l-phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 5 Abundance Scan 1098 (22.689 min): 12736.D (-) Tm/z 281.00 100.00% 21 11

5000

A 22.40 22.60 22.80 23.00 44 m/z 282.00 27.93% p-T-n-p-n-ry ■p m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39602: 6,7-Benzo-phenothiazine-5,5-dioxide 2I 1

wiilil 22.40 22.60 22.80 23.00 217 m/z 283.00 18.91% 232 102 118 189 , ,, j,|......264 I ' I ' ' ' ''i ‘ I'l I n-|-rri-i I I r 1 I p I Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39586: 1,2-Dihydroanthra[1,2-d]thiazole-2,6,11 -trione 2*1

22.40 22.60 22.80 23.00 5000 m/z 43.90 4.30%

209 253 76 127 153 170 ■ I " ' 11 ’’ Tl/Z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39624: 3,6-Bis(N-dimethylamino)-9-ethylcarbazole 21 11 22.40 22.60 22.80 23.00

5000 266

tt/z-2 40 60 80 141 I 208222^250 I ' I ’ ■ I ' ' ''r| ' I ' ' I 100 120 1^ 160 180 200 220 240 260 280 1

12736.D HP052902.M Mon Jun 03 19:58:14 2002 Page 3

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