VOC analysis results, sample AE12737, June 2002

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Data File C;\HPCHEM\l\DATA\02june3\12736.D Vial 5 Acq On 3 Jun 2002 7:18 pm Operator 201-wb Sample 524 Inst GC/MS Ins Mise Multiplr 1.00 MS Integration Params: LSCINT.P

Quant Method : C;\HPCHEM\1\METHODS\HP052902.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 N-(2-Acetylcyclopentylidene)cy Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 17.95 0.03 ug/L 28165 1,4-DIFLUOROBENZENE 15.11 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 N-(2-Acetylcyclopentylidene)cyclohe 207 C13H21NO 000000-00-0 9 2 Acetamide, N-[4-(trimethylsilyl)phe 207 CllH17NOSi 017983-71-0 7 3 Pyridot2,3-d]pyrimidine, 4-phenyl- 207 C13H9N3 028732-75-4 5 4 3-Methyl-2-phenylindole 207 C15H13N 010257-92^5 Abundance Scan 820 (17.953 min): 12736.D (-) m/z 206.95 100.00% 207

SEE [X ........ 96........................ 17.60 17.80 18.00 18.20 44 m/z 208.05 20.02% 'n/2-> 40 60 80 100 120 140 160 180 200 \ Abundance #24635: N-(2-Acetylcyclopentylidene)cyclohexyiamine 2(1)7

164 124 5000 17.60 17.80 18.00 18.20 82 97 IIO 150 m/z 95.90 17.90%

■n/2-> Abundance 40 60 XX-UX 80 100 120 140 160 180 192

200 #24586: Acetamide. N-[4-(trimethylsilyl)phenyl]- 192 207

I'''' I 17,60 17,80 18.00 18.20 m/z 43.85 4.03% 150

45 73 91 106 165 ' I i'' Tl/2-> 40 60 80 100 120 140 160 180 200 Abundance #24634; Pyrido[2,3-d]pyriinidine, 4-phenyl- 207 T 17.60 17.80 18.00 18.20

5000 179 77 , 103 152 , . ............. ....... . l| , 126 •n/z-> 40 60 80 100 120 140I 160 180 200

12736.D HP052902.M Mon Jun 03 19:58:12 2002 Page 2

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