VOC analysis results, sample AE12737, June 2002

NYC 9/11 Public Portal Document biCirary yearcn compouna Report

Data File C:\HPCHEM\l\DATA\02june3\12735.D Vial: 4 Acq On 3 Jun 2002 6:35 pm Operator: 201-wb Sample 524 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP052902.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peale Number 3 6,7-Benzo-phenothiazine-5,5-di Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 22.69 0.03 ug/L 27980 CHLOROBENZENE-D5 21.77 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 6,7-Benzo-phenothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0 5 2 l,2-Dihydroanthra[l,2-d]thiazole-2, 281 C15H7NO3S 000000-00-0 5 3 3,6-Bis(N-dimethylamino)-9-ethylcar 281 C18H23N3 057103-04-5 5 4 Benzene, l-phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 5 Abundance Scan 1098 (22.689 min): 12735.D (-) m/z 281.00 100.00% 2*1 Ir^ 5000

■R

Ti/z-> 44 40 60 133 I 1 22.40 22.60 22.80 23.00 m/z 282.00 28.30% 80 100 120 140 160 180 200 220 240 260 280 Abundance #39602: 6,7-Benzo-phenothiazine-5,5-dioxide 2$1

5000 22.40 22.60 22.80 23.00 217 m/z 283.00 19.95%

XX 232 102118 264 ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39586: 1,2-Dihydroanthra[1.2-d]thiazole-2,6,11 -trione 21 1

22.40 22.60 22.80 23.00 5000 m/z 132.90 16.55%

209 253 76 127 153 170 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39624: 3,6-Bis(N-dimethylamino)-9-ethylcarba2ole 2H1 ■n" 22.40 22.60 22.80 23.00 m/z 43.85 7.43%

5000 266

141 ocie250 20822224° I I Tp-TTT-p-lTTlYTT+p-rVTT ' r ''' I'''' I' tt/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 22.40 22.60 22.80 23.00

12735.D HP052902.M Mon Jun 03 19:15:24 2002 Page 3

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