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VOC analysis results, sample AE12738, June 4 2002

Machine-extracted title · confidence 100%

Laboratory report listing analytical results for volatile organic compounds in sample AE12738 analyzed on June 4, 2002.

NYC-WTC_000083874–000083923

Folder label: “524 6/4/02

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NYC 9/11 Public Portal Document LiJorary Search Compound Report

Data File C:\HPCHEM\l\DATA\02june04\12738A.D vial 8 Acq On 4 Jun 2002 6:23 pm Operator 201-wb Sample nyc Inst GC/MS Ins Mise Multiplr 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP052902.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L Sr**********************************************^,****^!****************

Peale Number 2 Benzene, l-phenyl-4-(2-cyano-2 Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 22.69 0.03 ug/L 34412 CHLOROBENZENE-D5 21.75 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Benzene, l-phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 5 2 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 4 3 6,7-Benzo-phenothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0. 3 4 1,2-Dihydroanthra[l,2-d]thiazole-2, 281 C15H7NO3S 000000-00-0 3 Abundance Scan 1098 (22.690 min); 12738A.D (-) m/z 281.00 100.00% 2fl1

5000

133 ......... (Vi..... Ti/z-> 40 44 I 60 80 100 120 140 160 180 200 220 240 260 280 I 22.40 22.60 22.80 23.00 m/z 282.10 34.76%

Abundance #39643: Benzene, 1-phenyl-4-(2-cyano-2-phenylethenyl) 2fi1

5000 22.40 22.60 22.80 23.00 __ 253 m/z 283.10 23.89% 126 J f/f I I, -n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #72646: Cyclotetrasiioxane, octamethyl- 2$1

22.40 22.60 22.80 23.00 5000 m/z 133.00 17.33%

73 265 45 59 I 133 lll2^flL235 '' I' ‘' I' ‘' I'''' I _L •n/z~> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39602: 6.7-Ben2O-phenothiazine-5,5-dioxide -n-p-r ' ' I ‘ ' 1 ' ' 281 22.40 22.60 22.80 23.00 m/z 43.85 0.47%

5000

217

tt/z-> 40 60 80 22121®. XX 100 120 140 160 180 200 220 240 260 280 232 264 1 r-pm-r-p 22.40 22.60 22.80 23.00

12738A.D HP052902.M Tue Jun 04 19:02:31 2002 Page 2

NYC-WTC_000083903

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NYC-WTC_000083903Source: NYC Law Department, mirrored locally

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