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VOC analysis results, sample AE12737, June 2002

Machine-extracted title · confidence 95%

Laboratory report for volatile organic compounds in sample AE12737 analyzed on June 3, 2002.

NYC-WTC_000083807–000083872

Folder label: “524 6/3/02

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Scanned page image, NYC-WTC_000083846
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NYC 9/11 Public Portal Document J_l CA J.

Data File C:\HPCHEM\l\DATA\02june3\12735.D Vial: 4 Acg On 3 Jun 2002 6:35 pm Operator: 201-wb Sample 524 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\HP052902.M {RTE Integrator) Title VOCs BY EPA METHOD 524 Library C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Hexahydropyridine, l-methyl-4- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 17.97 0.03 ug/L 27448 1,4-DIFLUOROBENZENE 15.11

Hit# of 5 Tentative ID MW. MolForm CAS# Qual

1 Hexahydropyridine, l-methyl-4-[4,5- 207 C12H17NO2 000000-00-0 9 2 Acetamide, N-[4-(trimethylsilyl)phe 207 CllH17NOSi 017983-71-0 7 3 Pyrido[2,3-d]pyrimidine, 4-phenyl- 207 C13H9N3 028732-75-4 5 4 N-Cyano-N',N',N'',N''-tetramethyl-1 207 C8H13N7 074150-88-2 5 Abundance Scan 821 (17.969 min): 12735.D (-) m/z 206.95 100.00% 2(1)7

5000 iX 96 17.60 17.80 18.00 18.20 44 m/z 207.95 20.44% 'n/z-> Abundance 40 60 80 100 120 140 160 180 200 #24610: Hexahydropyridine, 1-methyl-4-[4,5-dihydroxyphenyl]- A 2(1)7 70 42 97 lililil 82 17.60 17.80 18.00 18.20 m/z 96.00 18.70% 136 192 123 J 4^ ■n/z-> 40 60 80 100 120 140 160 180 200 Abundance #24586: Acetamide, N-[4-(trimethylsilyl)phenyi]- 192 2(1)7

17.60 17.80 18.00 18.20 liliW m/z 43.90 5.62% 150

45 73 91 106 165 m/z-> 40 60 80 100 120 140 160 180 200 Abundance #24634: Pyrido[2,3-d]pyrimidine, 4-phenyl- 207 17,60 17.80 18.00 18.20

5000 179 77

Tl/z-> 40 60 80 100 120 140 160 180 200

12735.D HP052902.M Mon Jun 03 19:15:22 2002 Page 2

NYC-WTC_000083846

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NYC-WTC_000083846Source: NYC Law Department, mirrored locally

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