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VOC analysis results, sample AE12738, June 4 2002

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Laboratory report listing analytical results for volatile organic compounds in sample AE12738 analyzed on June 4, 2002.

NYC-WTC_000083874–000083923

Folder label: “524 6/4/02

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NYC 9/11 Public Portal Document biOrary searcn compouna Keporc Data File C:\HPCHEM\l\DATA\02june04\12739A.D Vial: 9 Acq On 4 Jun 2002 7:06 pm Operator; 201-wb Sample nyc Inst : GC/MS Ins Mise Multiple: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP052902.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Hexahydropyridine, l-methyl-4- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 17.94 0.03 ug/L 24552 1,4-DIFLUOROBENZENE 15.09 Hit# of 5 Tentative ID MW MolFom CAS# Qual

1 Hexahydropyridine, l-methyl-4-[4,5- 207 C12H17NO2 000000-00-0 9 2 Pyrido[2,3-d]pyrimidine, 4-phenyl- 207 C13H9N3 028732-75-4 5 3 IH-Indole, 5-methyl-2-phenyl- 207 C15H13N 013228-36-9 5 4 4-Cyclohexene-l,2-dicarboximide, N- 207 C12H17NO2 028916-00-9 5 Abundance Scan 819 (17.936 min): 12739A.D (-) m/z 206.95 100.00% 207 8000

6000

4000 17.60 17.80 18.00 18.20

m/z-> 40 y 80 T 100 120 140 '160 180 200 m/z 96.00 26.79%

Abundance #24610: Hexahydropyridine, 1-methyl-4-[4,5-dihydroxyphenyl]- 2(1)7 70 42 97 5000 82 17.60 17.80 18.00 18.20 m/z 208.05 21.68% 136 123 [ 150 192 ................... I'C •n/z-> 40 60 80 100 120 140 160 180 200 Abundance #24634: Pyrido[2,3-d]pyrimidine. 4-phenyl- 2(1)7

17.60 17.80 18.00 18.20 5000 179 77 , 103

'n/z-> 40 60 80 100 120 140 160 180 200 Abundance #24654: IH-lndole, 5-methyl-2-phenyl- 2(17

5000

104 178 .............. l| , , 10^ 1^ II Tl/Z-> 40 60 80 100 120 140 160 180 200

12739A.D HP052902.M Tue Jun 04 19:45:31 2002 Page 2

NYC-WTC_000083909

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NYC-WTC_000083909Source: NYC Law Department, mirrored locally

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