VOC analysis results, sample AE12737, June 2002

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Data File C:\HPCHEM\l\DATA\02june3\12737.D Vial: 6 Acq On 3 Jun 2002 8:01 pm Operator; 201-wb Sample 524 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP052902.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ************************-********************************************* Peak Number 2 Hexahydropyridine, l-methyl-4- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 17.95 0.03 ug/L 27233 1,4-DIFLUOROBENZENE 15.11 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexahydropyridine, l-methyl-4-[4,5- 207 C12H17NO2 000000-00-0 9 2 Pyrido[2,3-d]pyrimidine, 4-phenyl- 207 C13H9N3 028732-75-4 5 3 lH-Isoindole-1, 3(2H)-dione, 2-butyl 207 C12H17NO2 ■ 054934-85-9 5 4 IH-Indole, l-methyl-2-phenyl-_________ 207 C15H13N 003558-24-5 5 Abundance Scan 820 (17.953 min): 12737.D {-) m/z 206.95 100.00% 247

5000

96 17.60 17.80 18.00 18.20 44 m/z 207.95 20.69% Ti/z-> 40 60 80 100 120 140 160 180 200 A Abundance #24610; Hexahydropyridine. 1-methyl-4-[4,5-dihydroxyphenyl]- 207 70 42 97 5000 I 82 17.60 17.80 18.00 18.20 m/z 96.00 18.62% 136 192 Ti/z-> 40 60 80 100 120 As123 160 180 200 140 Abundance #24634: Pyrido[2,3-d]pyrimidine, 4-phenyl- 207

nA 17.60 17.80 18.00 18.20 5000 m/z 43.90 10.69% 179 77 1.^11^21 'n/z-> 40 60 80 100 120 140 160 180 200 - ------------------------- --------------------- -------—----- -—xzZ Abundance #24616: 1H-lsoindole-1,3(2H)-dione. 2-butyl-4,5,6,7-tetrahy 2(1)7 17.60 17,80 18.00 18.20 79

5000 152 165

■n/z-> 40 60 80 100 111 124 136 120 . 140 160 180 200 L

12737.D HP052902.M Mon Jun 03 20:40:52 2002 Page 2

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