VOC analysis results, sample AE12737, June 2002

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Data File C:\HPCHEM\l\DATA\02june3\12737.D Vial: 6 Acq On 3 Jun 2002 8:01 pm Operator: 201-wb Sample 524 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\HP052902.M (RTE Integrator) Title VOCs BY EPA METHOD 524 Library C:\DATABASE\NBS75K.L ***-****************************************************************** Peak Number 3 6,7-Benzo-phenothiazine-5,5-di Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 22.69 0.03 ug/L 27887 CHLOROBENZENE-D5 21.77 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 6,7-Benzo-phenothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0 5 2 l,2-Dihydroanthra[l,2-d]thiazole-2, 281 C15H7NO3S 000000-00-0 5 3 3,6-Bis(N-dimethylamino)-9-ethylcar 281 C18H23N3 057103-04-5 5 4 Benzene, l-phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 5 Abundance Scan 1098 (22.689 min): 12737.D (-) m/z 281.00 100.00% 2*1

5000

133 22.40 22.60 22.80 23.00 44 I ' ' ' I ‘ ' ’1”' ' ' ' I ' ■ ' ' I ' ' ' I -p-m-p-n-q-T m/z 282.00 26.38% •n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39602: 6,7-Benzo-phenothiazine-5,5-dioxide 2*1

OWil 22.40 22.60 22.80 23.00 217 m/z 283.00 18.92% I 232 102 118 264 1 ' I'''' I'''' I' ' I '' ' 'I ' I ' ' ' ' I r-p-r-n-p •n/z--> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39586: 1,2-Dihydroanthra[1,2-d]thiazole-2,6,11-trione 21 4

22.40 22.60 22.80 23.00 lililil m/z 132.90 17.12%

209 253 76 127 153 170 'hr 'n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39624: 3,6-Bis(N-dimethylamino)-9-ethylcarbazole 2*1 22.40 22.60 22.80 23.00 m/z 43.85 5.71%

5000 266

141 208222236^1° I m/2-> 40 60 80 100 120 140 160 180 200 220 240 260 280 22.40 22.60 22.80 23.00

12737.D HP052902.M Mon Jun 03 20:40:55 2002 Page 3

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