VOC analysis results, sample AE12737, June 2002

NYC 9/11 Public Portal Document yuarici caciuii nepur c iwoc Kevieweu; Data File C:\HPCHEM\l\DATA\02JUNE3\0603C10.D Vial 4 Acq On 3 Jun 2002 11:42 am Operator 201-wb Sample cal 10 Inst GC/MS Ins Mise Multiplr 1.00 MS Integration Params: GAS6.P Quant Time: Jun 3 13:32 2002 Quant Results File: HP052902.RES Quant Method : C:\HPCHEM\1\METHODS\HP052902.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Fri May 31 14:34:13 2002 Response via : Initial Calibration DataAcq Meth : HP052902

Internal Standards R.T. Qlon- Response Cone Units Dev(Min) 1) 1,4-DIFLUOROBENZENE 15.09 114 1693806 5.00 ug/L -0.02 24) CHLOROBENZENE-D5 21.75 117 1553058 5.00 ug/L 0.00 52) 1,4-DICHLOROBENZENE-D4 26.93 152 821070 5.00 ug/L 0.00 System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 14.32 65 698312 4.56 ug/L -0.02 Spiked TUnount 5.000 Recovery = 91.20% 3) 4-BROMOFLUOROBENZENE 24.33 174 638220 4.73 ug/L -0.02 Spiked Amount 5.000 Recovery = 94.60% 25) TOLUENE-D8 18.45 98 2025001 5.17 ug/L -0.02 Spiked Amount 5.000 Recove3ry = 103.40% Target Compounds Qvalue 4) DICHLORODIFLUOROMETHANE 4.85 85 609705 10.08 ug/L 99 5) CHLOROMETHANE 5.35 50 777071 8.28 ug/L 99 6) VINYL CHLORIDE 5.59 62 495415 10.19 ug/L 97 7) BROMOMETHANE 6.56 94 300536 11.33 ug/L 99 8) CHLOROETHTkNE 6.70 64 446932 10.26 ug/L 97 9) TRICHLOROFLUOROMETHANE 7.27 101 830891 11.53 ug/L 98 10) Isopropyl Alcohol 7.87 45 298897 190.43 ug/L 100 11) 1,1,2-Trichloro-l, 2,2-trif 8.16 101 533735 9.66 ug/L 98 12) ACETONE 8.22 43 354771 20.07 ug/L 99 13) 1,1-dichlOroethene 8.58 61 1047706 8.60 ug/L 98 14) METHYLENE CHLORIDE 9.59 49 928203 8.20 ug/L 95 15) METHYL TERT BUTYL ETHER 9.89 73 733711 8.38 ug/L 95 16) TRANS-1,2-DICHLOROETHENE 10.25 61 1120939 8.96 ug/L 93 17) 1,1-DICHLOROETHANE 11.15 63 1229438 8.77 ug/L 98 18) 2-BUTANONE (MEK) 11.97 43 413775 31.28 ug/L 96 19) 2,2-DICHLOROPROPANE 12.36 77 980015 9.37 ug/L 97 20) CIS-1,2-DICHLOROETHENE 12.47 96 718672 9.79 ug/L 85 21) CHLOROFORM 12.79 83 1348843 9.36 ug/L 99 22) BROMOCHLOROMETHANE 13.17 49 510200 8.25 ug/L 91 23) 1,2-DICHLOROETHANE 14.51 62 890458 8.86 ug/L 100 26) 1,1,1-TRICHLOROETHANE 13.69 97 1065625 10.60 ug/L 99 27) 1,1-DICHLOROPROPENE 14.02 75 1011030 10.66 ug/L 97 28) CARBON TETRACHLORIDE 14.27 117 926088 11.04 ug/L 99 29) BENZENE 14.61 78 2388503 10.28 ug/L 100 30) TRICHLOROETHENE 15.89 95 751098 10.79 ug/L 94 31) 1,2-DICHLOROPROPANE 16.25 63 582931 9.54 ug/L 98 32) DIBROMOMETHANE 16.91 174 312955 11.12 ug/L 94 33) BROMODICHLOROMETHANE 16.76 83 901849 10.31 ug/L 98 34) 2-CHLOROETHYL VINYL ETHER 17.25 63 175111 9.70 ug/L 85 35) METHYL ISO-BUTYL KETONE 17.32 58 348920 40.35 ug/L 96 36) CIS-1,3-DICHLOROPROPENE 17.85 75 825287 10.29 ug/L 99 37) TOLUENE 18.62 91 2512677 10.36 ug/L 97 38) TRANS-1,3-DICHLOROPROPENE 18.89 75 582553 10.14 ug/L 98 39) 1,1,2-TRICHLOROETHANE 19.28 97 364352 10.21 ug/L 98 4 0) TETRACHLOROETHENE 20.07 166 770534 11.51 ug/L 98 41) 1,3-DICHLOROPROPANE 19.81 76 691033 9.89 ug/L 100 42) DIBROMOCHLOROMETHANE 20.51 129 4792’09 11.02 ug/L 100 43) 1,2-DIBROMOETHANE 20.95 107 363930 10.28 ug/L 94 44) CHLOROBENZENE 21.84 112 1636375 10.65 ug/L 94 45) 1,1,1,2-TETRACHLOROETHANE 21.87 131 561214 10.96 ug/L 98 46) 2-HEXANONE 19.18 43 652032 38.67 ug/L 99 (#) = qualifier out of range (m) = manual integration 0603C10.D HP052902.M Mon Jun 03 13:32:15 2002 Page 1

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