Volatile organic compounds blank analysis results, March 22, 2002

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed) Data File : C:\HPCHEM\1 \DATA\ mar22\0322C10A.D Vial: 2 Acq On : 22 Mar 2002 9:23 pin Operator: 201-wb Sample : cal 10 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 22 22:01 2002 Quant Results File: HP031802.RES Quant Method : C:\HPCHEM\1\METHODS\HP031802.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Fri Mar 22 14:32:26 2002 Response via : Initial Calibration DataAcq Meth : HP031802

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-DIFLUOROBENZENE 15.08 114 919408 5.00 ug/L 0.03 24) CHLOROBENZENE-D5 21.74 117 873054 5.00 ug/L 0.03 52) 1,4-DICHLOROBENZENE-D4 26.92 152 476210 5.00 ug/L 0.03 System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 14.32 65 447713 5.91 ug/L 0.03 Spiked Amount 5.000 Recovery = 118.20% 3) 4-BROMOFLU0ROBENZENE 24.33 174 383308 5.16 ug/L 0.03 Spiked Amount• 5.000 Recovery = 103.20% 25) TOLUENE-D8 18.44 98 1085082 5.13 ug/L 0.03 Spiked Amount 5.000 Recovery = 102.60% Target Compounds Qvalue 4) DICHLORODIFLUOROMETHANE 4.83 85 256116 9.38 ug/L 99 5) CHLOROMETHANE 5.45 50 323498 9.84 ug/L 94 6) VINYL CHLORIDE 5.57 62 252275 13.91 ug/L 96 7) BROMOMETHANE 6.56 94 258971 11.86 ug/L 97 8) CHLOROETHANE 6.69 64 245814 10.90 ug/L 99 9) TRICHLOROFLUOROMETHANE 7.25 101 513229 11.20 ug/L 98 10) Isopropyl Alcohol 7.87 45 15444 17.70 ug/L 98 11) l,l,2-Trichloro-l,2,2-trif 8.12 101 6129 0.30 ug/L 87 12) ACETONE 8.22 43 218724 41.09 ug/L 98 13) 1,1-DICHLOROETHENE 8.58 61 469643 8.55 ug/L 100 14) METHYLENE CHLORIDE 9.59 49 453914 9.30 ug/L 99 15) METHYL TERT BUTYL ETHER 9.89 73 601821 12.20 ug/L 100 16) TRANS-1,2-DICHLOROETHENE 10.25 61 513195 9.30 ug/L 97 17) 1,1-DICHLOROETHANE 11.14 63 592107 9.36 ug/L 99 18) 2-BUTANONE (MEK) 11.97 43 239915 35.48 ug/L 99 19) 2,2-DICHLOROPROPANE 12.36 77 455187 9.24 ug/L 96 20) CIS-1,2-DICHLOROETHENE 12.46 96 373863 10.06 ug/L 95 21) CHLOROFORM 12.79 83 727540 10.64 ug/L 100 22) BROMOCHLOROMETHANE 13.16 49 267234 9.41 ug/L 96 23) 1,2-DICHLOROETHANE 14.51 62 518400 10.97 ug/L 99 26) 1,1,1-TRICHLOROETHANE 13.69 97 555023 11.26 ug/L 98 27) 1,1-DICHLOROPROPENE 14.01 75 448049 9.88 ug/L 98 28) CARBON TETRACHLORIDE 14.27 117 490414 11.55 ug/L 100 29) BENZENE 14.61 78 1114283 9.87 ug/L 98 30) TRICHLOROETHENE 15.89 95 371580 10.53 ug/L 98 31) 1,2-DICHLOROPROPANE 16.24 63 287801 9.76 ug/L 96 32) DIBROMOMETHANE 16.92 174 189775 11.35 ug/L 86 33) BROMODICHLOROMETHANE 16.75 83 502850 11.26 ug/L 99 34) 2-CHLOROETHYL VINYL ETHER 17.25 63 112995 9.60 ug/L 92 35) METHYL ISO-BUTYL KETONE 17.32 58 208364 41.38 ug/L 88 36) CIS-1,3-DICHLOROPROPENE 17.84 75 430889 10.08 ug/L 98 37) TOLUENE 18.61 91 1238956 10.24 ug/L 97 3 8) TRANS-1,3-DICHLOROPROPENE 18.88 75 338211 10.72 ug/L 97 39) 1,1,2-TRICHLOROETHANE 19.27 97 211904 10.61 ug/L 95 40) TETRACHLOROETHENE 20.06 166 386388 10.79 ug/L 99 41) 1,3-DICHLOROPROPANE 19.80 76 378226 10.28 ug/L 95 42) DIBROMOCHLOROMETHANE 20.50 129 298018 11.56 ug/L 97 43) 1,2-DIBROMOETHANE 20.94 107 214766 10.54 ug/L 97 44) CHLOROBENZENE 21.83 112 857500 10.52 ug/L 100 45) 1,1,1,2-TETRACHLOROETHANE 21.88 131 330256 11.48 ug/L 96 46) 2-HEXANONE 19.17 43 381743 40.96 ug/L 96 (#) = qualifier out of range (m) = manual integration 0322C10A.D HP031802.M Fri Mar 22 22:01:51 2002 Page 1

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