Volatile organic compounds analysis results, March 25, 2002

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

Data File : C: \HPCHEM\1\DATA\02MAR25\0325C10A.D Vial: 2 Acq On : 25 Mar 2002 9:55 pm Operator: 201-wb Sample : cal 10 Inst : GC/MS Ins Mise & Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 26 8:15 2002 Quant Results File: HP031802.RES Quant Method : C:\HPCHEM\1\METHODS\HP031802.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Mon Mar 25 15:09:58 2002 Response via : Initial Calibration DataAcq Meth : HP031802

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-DIFLUOROBENZENE 15.03 114 1239206 5.00 ug/L -0.02 24) CHLOROBENZENE-D5 21.69 117 1204363 5.00 ug/L -0.02 52) 1,4-DICHLOROBENZENE-D4 26.87 152 689670 5.00 ug/L -0.02

System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 14.27 65 612112 6.00 ug/L -0.02 Spiked Amount 5,000 Recovery = 120.00% 3) 4-BROMOFLUOROBENZENE 24.28 174 560222 ■ 5.59 ug/L -0.02 Spiked Amount 5.000 Recovery = 111.80% 25) TOLUENE-D8 18.39 98 1475715 5.06 ug/L -0.02 Spiked Amount 5.000 Recovery = 101.20% Target Compounds Qvalue 4) DICHLORODIFLUOROMETHANE 4.81 85 504340 13.70 ug/L 100 5) CHLOROMETHANE 5.43 50 477441 10.77 ug/L 94 6) VINYL CHLORIDE 5.55 62 416747 13.31 ug/L 100 7) BROMOMETHANE 6.52 94 331643 11.27 ug/L 97 8) CHLOROETHANE 6.66 64 328739 10.82 ug/L 98 9) TRICHLOROFLUOROMETHANE 7.21 101 711655 11.52 ug/L 99 11) 1,1,2-Trichloro-l,2,2-trif 8.11 101 10811 0.40 ug/L 91 12) ACETONE 8.19 43 296276 41.32 ug/L 99 13) 1,1 -.DICHLOROETHENE 8.55 61 . 796912 10.76 ug/L 98 14) METHYLENE CHLORIDE 9.54 49 636010 9.67 ug/L 99 15) METHYL TERT BUTYL ETHER 9.86 73 676504 10.17 ug/L 98 16) TRANS-1,2-DICHLOROETHENE 10.22 61 751889 10.11 ug/L 97 17) 1,1-DICHLOROETHANE 11.10 63 857211 10.06 ug/L 97 18) 2-BUTANONE (MEK) 11.94 43 313806 34.43 ug/L 96 19) 2,2-DICHLOROPROPANE 12.31 77 650759 9.78 ug/L 94 20) CIS-1,2-DICHLOROETHENE 12.41 96 528869 10.56 ug/L 97 21) CHLOROFORM 12.75 83 1018970 11.05 ug/L 97 2 2) BROMOCHLOROMETHANE. 13.13 49 361581 9.45 ug/L 88 23) 1,2-DICHLOROETHANE 14.47 62. 739025 11.60 ug/L 99 26) 1,1,1-TRICHLOROETHANE 13.64 97 843014 12.39 ug/L 97 27) 1,1-DICHLOROPROPENE 13.96 75 675424 10.80 ug/L 98 28) CARBON TETRACHLORIDE 14.23 117 759612 12.97 ug/L 98 29) BENZENE 14.57 78 1575990 10.12 ug/L 99 30) TRICHLOROETHENE 15.83 95 529412 10.87 ug/L 97 31) 1,2-DICHLOROPROPANE 16.19 63 386641 9.50 ug/L 98 3 2) DIBROMOMETHANE 16.87 174 278984 12.10 ug/L 91 33) BROMODICHLOROMETHANE 16.72 83 705185 11.45 ug/L 99 34) 2-CHLOROETHYL VINYL ETHER 17.20 63 150999 9.30 ug/L 100 35) METHYL ISO-BUTYL KETONE 17.28 58 272582 39.25 ug/L 96 36) CIS-1,3-DICHLOROPROPENE 17.81 ' 75 592450 10.04 ug/L 99 3 7) TOLUENE 18.56 91 1734366 10.39 ug/L 98 38) TRANS-1,3-DICHLOROPROPENE 18.85 75. 459650 10.56 ug/L . 99 39) 1,1,2-TRICHLOROETHANE 19.22 97 294762 10.70 ug/L 96 40) TETRACHLOROETHENE 20.01 166 572153 11.58 ug/L 99 41) 1,3-DICHLOROPROPANE 19.77 76 516417 10.17 ug/L 97 42) DIBROMOCHLOROMETHANE 20.45 129 419766 11.80 ug/L 97 43) 1,2-DIBROMOETHANE 20.89 107 309064 11.00 ug/L 98 44) CHLOROBENZENE 21.78 112 1180945 10.50 ug/L ■ 97 45) 1,1,1,2-TETRACHLOROETHANE 21.83 131 464964 11.71 ug/L 95 46) 2-HEXANONE 19.12 43 503422 39.15 ug/L 95 47) ETHYLBENZENE 21.81 91 2092002 10.78 ug/L 97 (#) = qualifier out of range (m) = manual integration 0325C10A.D HP031802.M Tue Mar 26 08:15:14 2002 ■ Page 1

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