Volatile organic compounds blank analysis results, March 22, 2002

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed) Data File : C:\HPCHEM\1\DAT.02mar22\0322C10B.D Vial: 2 Acq On : 23 Mar 2002 3:53 om Operator: 201-wb Sample : cal 10 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 23 4:32 2002 Quant Results File: HP031802.RES Quant Method : C:\HPCHEM\1\METHODS\HP031802.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Fri Mar 22 14:32:26 2002 Response via : Initial Calibration DataAcq Meth : HP031802

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-DIFLUOROBENZENE 15.08 114 972029 5.00 ug/L 0.03 24) CHLOROBENZENE-D5 21.74 117 926829 5.00 ug/L 0.03 52) 1,4-DICHLOROBENZENE-D4 26.92 152 499393 5.00 ug/L 0.03 System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 14.32 65 477228 5.96 ug/L 0.03 Spiked Amount 5.000 Recovery = 119.20% 3) 4-BROMOFLU0ROBENZENE 24.31 174 406473 5.17 ug/L 0.02 Spiked Amount• 5.000 Recovery = 103.40% 25) TOLUENE-D8 18.44 98 1146429 5.11 ug/L 0.03 Spiked Amount 5.000 Recovery = 102.20% Target Compounds Qvalue 4) DICHLORODIFLUOROMETHANE 4.83 85 268772 9.31 ug/L 96 5) CHLOROMETHANE 5.45 50 345856 ug/L 98 6) VINYL CHLORIDE 5.57 62 292694 1 ug/L 100 7) BROMOMETHANE 6.56 94 263551 11.42 ug/L 98 8) CHLOROETHANE 6.69 64 251907 10.57 ug/L 99 9) TRICHLOROFLUOROMETHANE 7.25 101 528893 10.92 ug/L 96 10) Isopropyl Alcohol 7.87 45 16362 — 17.74 ug/L 95 11) l,l,2-Trichloro-l,2,2-trif 8.16 101 6670 0.31 ug/L 90 12) ACETONE 8.22 43 237414 --42.31 ug/L 96 13) 1,1-DICHLOROETHENE 8.58 61 520187 8.95 ug/L 99 14) METHYLENE CHLORIDE 9.59 49 473375 9.17 ug/L 98 15) METHYL TERT BUTYL ETHER 9.89 73 501606 9.62 ug/L 99 16) TRANS-1,2-DICHLOROETHENE 10.25 61 534903 9.17 ug/L 97 17) 1,1-DICHLOROETHANE 11.14 63 625956 9.36 ug/L 96 18) 2-BUTANONE (MEK) 11.97 43 247999 — 34.69 ug/L 99 19) 2,2-DICHLOROPROPANE 12.36 77 404607 7.81 ug/L 95 20) CIS-1,2-DICHLOROETHENE 12.45 96 387928 9.87 ug/L 97 21) CHLOROFORM 12.79 83 769977 10.65 ug/L 96 22) BROMOCHLOROMETHANE 13.16 49 278561 9.28 ug/L 99 23) 1,2-DICHLOROETHANE 14.51 62 551006 11.03 ug/L 99 26) 1,1,1-TRICHLOROETHANE 13.69 97 597083 11.41 ug/L 98 27) 1,1-DICHLOROPROPENE 14.01 75 484720 10.07 ug/L 99 28) CARBON TETRACHLORIDE 14.27 117 533635 11.84 ug/L 99 29) BENZENE 14.61 78 1175063 9.80 ug/L 99 30) TRICHLOROETHENE 15.88 95 391154 10.44 ug/L 97 31) 1,2-DICHLOROPROPANE 16.24 63 297453 9.50 ug/L 98 32) DIBROMOMETHANE 16.91 174 201305 11.34 ug/L 96 33) BROMODICHLOROMETHANE 16.75 83 528003 11.14 ug/L 99 34) 2-CHLOROETHYL VINYL ETHER 17.25 63 115773 9.27 ug/L 93 35) METHYL ISO-BUTYL KETONE 17.32 58 216190 .— 40.45 ug/L 93 36) CIS-1,3-DICHLOROPROPENE 17.84 75 443965 9.78 ug/L 98 37) TOLUENE 18.61 91 1308611 10.19 ug/L 99 38) TRANS-1,3-DICHLOROPROPENE 18.88 75 341845 10.21 ug/L 97 39) 1,1,2-TRICHLOROETHANE 19.27 97 223489 10.54 ug/L 95 40) TETRACHLOROETHENE 20.06 166 414298 10.90 ug/L 98 41) 1,3-DICHLOROPROPANE 19.80 76 401736 10.28 ug/L 95 42) DIBROMOCHLOROMETHANE 20.50 129 318450 11.63 ug/L 100 43) 1,2-DIBROMOETHANE 20.94 107 227702 10.53 ug/L 96 44) CHLOROBENZENE 21.83 112 902002 10.42 ug/L 98 45) 1,1,1,2-TETRACHLOROETHANE 21.86 131 350331 11.47 ug/L 97 46) 2-HEXANONE 19.17 43 396989 — 40.12 ug/L 92 (#) = qualifier out of range (m) = manual integration 0322C10B.D HP031802.M Sat Mar 23 04:32:19 2002 Page 1

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