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Volatile organic compound analysis results, sample AE08951, April 2002

Machine-extracted title · confidence 100%

Laboratory report listing volatile organic compounds and concentrations for sample AE08951 with method detection limit qualifiers.

NYC-WTC_000082119–000082220

Folder label: “524 4/19/02

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NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

Data File : C:\HPCHEM\l\DATA\02aprl9\0419C10.D Vial: 2 Acq On : 19 Apr 2002 11:00 am Operator: 201-wb Sample : cal 10 Inst : GC/MS Ins Mise :,April 19, 2002 Multiplr; 1.00 MS Integration Params: RTEINT.P Quant Time: Apr 19 11:38 2002 Quant Results File: HP031802.RES

Quant Metliod C:\HPCHEM\1\METHODS\HP031802.M (RTE Integrator) Title VOCs BY EPA METHOD 524 Last Update Mon Apr 15 10:00:49 2002 Response via Initial Calibration DataAcq Meth HP031802

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-DIFLUOROBENZENE 15.10 114 1238469 5.00 ug/L 0.05 24) CHLOROBENZENE-D5 21.78 117 1118317 5.00 ug/L 0.07 52) 1,4-DICHLOROBENZENE-D4 26.97 152 544624 5.00 ug/L 0.09

System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 14.34 65 602238 5.90 ug/L 0.05 Spiked Amount 5.000 Recovery = 118.00% 3) 4-BROMOFLUOROBENZENE 24.36 174 444749 4.44 ug/L 0.07 Spiked Amount 5.000 Recovery = 88.80% 25) TOLUENE-D8 18.47 98 1459642 5.39 ug/L 0.07 Spiked Amount 5.000 Recovery = 107.80%

Target Compounds Qvalue 4) DICHLORODIFLUOROMETHANE 4.87 85 356550 8.71 ug/L 99 5) CHLOROMETHANE 5.47 50 452996 9.27 ug/L 97 6) VINYL CHLORIDE 5.60 • 62 361521 11.55 ug/L 98 7) BROMOMETHANE 6.59 94 304478 10.36 ug/L 99 8) CHLOROETHANE 6.73 64 316317 10.42 ug/L 98 9) TRICHLOROFLUOROMETHANE 7.28 101 551422 9.53 ug/L 97 11) 1,1,2-Trichloro-l, 2,2-trif 8.17 101 8128 'KCjTl^g/L 73 12) ACETONE 8.26 43 302670 ' 35712 ug/L 96 13) 1,1-DICHLOROETHENE 8.62 61 764963 10.34 ug/L 92 14) METHYLENE CHLORIDE 9.62 49 703165 10.69 ug/L 93 15) METHYL TERT BUTYL ETHER 9.91 73 514417 .7.74 ug/L 94 16) TRTkNS-l, 2-DICHLOROETHENE 10.28 61 784576 10.56 ug/L 91 17) 1,1-DICHLOROETHANE 11.17 63 865431 10.16 ug/L 98 18) 2-BUTANONE (MEK) 12.00 43 327807 --.35.99 ug/L 96 19) 2,2-DICHLOROPROPANE 12.40 77 675557 10.08 ug/L 94 20) CIS-1,2-DICHLOROETHENE 12.48 96 475771 9.50 ug/L 88 21) CHLOROFORM 12.82 83 916444 9.95 ug/L 100 22) BROMOCHLOROMETHANE 13.20 49 383292 10.02 ug/L 82 23) 1,2-DICHLOROETKANE 14.54 62 659398 10.36 ug/L 97 26) 1,1,1-TRICHLOROETHANE 13.71 97 692611 10.97 ug/L 98 27) 1,1-DICHLOROPROPENE 14.03 75 656325 11.30 ug/L 96 28) CARBON TETRACHLORIDE 14.30 117 606087 11.15 ug/L 100 29) BENZENE 14.64 78 1559741 10.78 ug/L 99 30) TRICHLOROETHENE 15.92 95 477656 10.57 ug/L 99 31) 1,2-DICHLOROPROPANE 16.28 63 398040 10.54 ug/L 98 32) DIBROMOMETHANE 16.94 174 199813 9.33 ug/L 92 33) BROMODICHLOROMETHANE 16.79 83 610408 10.67 ug/L 99 34) 2-CHLOROETHYL VINYL ETHER 17.26 63 136811 8.51 ug/L 94 35) METHYL ISO-BUTYL KETONE 17.35 58 248341 —-38.51 ug/L 89 36) CIS-1,3-DICHLOROPROPENE 17.88 75 550377 10.05 ug/L 97 37) TOLUENE 18.64 91 1553694 10.03 ug/L 99 3 8) TRANS-1,3-DICHLOROPROPENE 18.92 75 398100 9.85 ug/L 94 39) 1,1,2-TRICHLOROETHANE 19.31 97 234371 9.16 ug/L 97 40) TETRACHLOROETHENE 20.09 166 449338 9.79 ug/L 99 41) 1,3-DICHLOROPROPANE 19.84 76 466079 9.89 ug/L 99 42) DIBROMOCHLOROMETHANE 20.53 129 303705 9.19 ug/L 98 43) 1,2-DIBROMOETH7V1E 20.98 107 233035 8.93 ug/L 97 44) CHLOROBENZENE 21.86 112 978914 9.38 ug/L 89 45) 1,1,1,2-TETRACHLOROETHANE 21.91 131 359141 9.74 ug/L 97 46) 2-HEXANONE 19.19 43 486340 _ ;40.74 ug/L 93 4 7) ETHYLBENZ ENE 21.90 91 1866596 10.36 ug/L 96

(#) = qualifier out of range (m) = manual integration 0419C10.D HP031802.M Fri Apr 19 11:38:59 2002 Page 1

NYC-WTC_000082127

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NYC-WTC_000082127Source: NYC Law Department, mirrored locally

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