Volatile organic compounds blank analysis results, March 22, 2002

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

Data File : C:\HPCHEM\1\DATA\02mar22\0322C10.D Vial: 2 Acq On : 22 Mar 2002 10:06 am Operator: 201-wb Sample : cal 10 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 22 10:44 2002 Quant Results File: HP031802.RES

Quant Method : C:\HPCHEM\1\METHODS\HP031802.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Fri Mar 22 09:11:28 2002 Response via : Initial Calibration DataAcq Meth : HP031802

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-DIFLUOROBENZENE 15.08 114 1103527 5.00 ug/L 0.03 24) CHLOROBENZENE-D5 21.74 117 1017080 5.00 ug/L 0.03 52) 1,4-DICHLOROBENZENE-D4 26.92 152 570148 5.00 ug/L 0.03

System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 14.32 65 511702 5.63 ug/L 0.03 Spiked Amount 5.000 Recovery = 112.60% 3) 4-BROMOFLUOROBENZENE 24.33 174 450275 5.05 ug/L 0.03 Spiked Amount 5.000 Recovery = 101.00% 25) TOLUENE-D8 18.44 98 1286377 5.22 ug/L 0.03 Spiked Amount 5.000 Recovery = 104.40%

Target Compounds Qvalue 4) DICHLORODIFLUOROMETHANE 4.83 85 259881 7.93 ug/L 99 5) CHLOROMETHANE 5.47 50 333012 8.46 ug/L 99 6) VINYL CHLORIDE 5.57 62 279054 11.89 ug/L 99 7) BROMOMETHANE 6.56 94 248328 9.48 ug/L 99 8) CHLOROETHANE 6.69 64 266984 9.87 ug/L 97 9) TRICHLOROFLUOROMETHANE 7.25 101 592210 10.77 ug/L 99 10) Isopropyl Alcohol 7.85 45 16749 16.00 ug/L 97 11) 1,1,2-Trichloro-l, 2,2-trif 8.14 101 8212 0.34 ug/L 98 12) ACETONE 8.22 43 253139 39.46 ug/L 96 13) 1,1-DICHLOROETHENE 8.56 61 602680 9.14 ug/L 97 14) METHYLENE CHLORIDE 9.59 49 506653 8.65 ug/L 95 15) METHYL TERT BUTYL ETHER 9.89 73 553691 9.35 ug/L 98 16) TRANS-1,2-DICHLOROETHENE 10.25 61 615260 9.29 ug/L 99 17) 1,1-DICHLOROETHANE 11.13 63 701419 9.24 ug/L 98 18) 2-BUTANONE (MEK) 11.97 43 281685 34.71 ug/L 100 19) 2,2-DICHLOROPROPANE 12.36 77 623903 10.44 ug/L 95 20) CIS-1,2-DICHLOROETHENE 12.45 96 433425 9.72 ug/L 98 21) CHLOROFORM 12.79 83 832955 10.15 ug/L 98 22) BROMOCHLOROMETHANE 13.16 49 299619 8.79 ug/L 98 23) 1,2-DICHLOROETHANE 14.51 62 597264 10.53 ug/L 96 26) 1,1,1-TRICHLOROETHANE 13.69 97 680431 11.84 ug/L 98 27) 1,1-DICHLOROPROPENE 14.01 75 574779 10.88 ug/L 98 28) CARBON TETRACHLORIDE 14.27 117 621066 12.56 ug/L 100 29) BENZENE 14.61 78 1303325 9.91 ug/L 99 30) TRICHLOROETHENE 15.88 95 448237 10.90 ug/L 97 31) 1,2-DICHLOROPROPANE 16.24 63 325516 9.48 ug/L 99 32) DIBROMOMETHANE 16.91 174 216547 11.12 ug/L 95 33) BROMODICHLOROMETHANE 16.75 83 585775 11.26 ug/L 99 34) 2-CHLOROETHYL VINYL ETHER 17.25 63 134773 9.83 ug/L 97 35) METHYL ISO-BUTYL KETONE 17.31 58 235243 40.11 ug/L 93 36) CIS-1,3-DICHLOROPROPENE 17.86 75 517306 10.38 ug/L 99 37) TOLUENE 18.61 91 1467429 10.41 ug/L 97 38) TRANS-1,3-DICHLOROPROPENE 18.88 75 403529 10.98 ug/L 96 39) 1,1,2-TRICHLOROETHANE 19.27 97 239732 10.30 ug/L 98 40) TETRACHLOROETHENE 20.06 166 483139 11.58 ug/L 97 41) 1,3-DICHLOROPROPANE 19.80 76 432818 10.09 ug/L 97 42) DIBROMOCHLOROMETHANE 20.50 129 351236 11.69 ug/L 96 43) 1,2-DIBROMOETHANE 20.94 107 253881 10.70 ug/L 99 44) CHLOROBENZENE 21.83 112 995053 10.48 ug/L 99 45) 1,1,1,2-TETRACHLOROETHANE 21.88 131 391204 11.67 ug/L 97 46) 2-HEXANONE 19.17 43 446423 41.11 ug/L 96

(#) = qualifier out of range (m) = manual integration 0322C10.D HP031802.M Fri Mar 22 10:45:07 2002 Page 1

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