Volatile organic compounds analysis results, March 21, 2002

NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\1\DATA\02MAR21\0321C10A.D Vial: 2 Acq On : 21 Mar 2002 9:24 pm Operator: 201-wb Sample : cal 10 Inst : GC/MS Ins Mise : March 21, 2002 Multiple: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 22 9:11 2002 Quant Results File: HP031802.RES Quant Method : C:\HPCHEM\1\METHODS\HP031802.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Fri Mar 22 09:11:28 2002 Response via : Initial Calibration DataAcq Meth : HP031802

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-DIFLUOROBENZENE 15.14 114 937441 5.00 ug/L 0.09 24) CHLOROBENZENE-D5 21.79 117 764100 5.00 ug/L 0.09 52) 1,4-DICHLOROBENZENE-D4 26.97 152 399528 5.00 ug/L 0.09 System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 14.37 65 469116 6.07 ug/L 0.09 Spiked Amount 5.000 Recovery = 121.40% 3) 4-BROMOFLUOROBENZENE 24.38 174 319831 4.22 ug/L 0.09 Spiked Amount 5.000 Recovery = 84.40% 25) TOLUENE-D8 18.49 98 967281 5.23 ug/L 0.09 Spiked Amount 5.000 Recovery = 104.60% Target Compounds Qvalue 4) DICHLORODIFLUOROMETHANE 4.86 85 178790 6.42 ug/L ✓ 97 5) CHLOROMETHANE 5.48 50 280142 8.38 ug/L 97 6) VINYL CHLORIDE 5.60 62 200430 9.15 ug/L 97 7) BROMOMETHANE 6.59 94 246107 11.06 ug/L 97 8) CHLOROETHANE 6.74 64 221974 9.66 ug/L 99 9) TRICHLOROFLUOROMETHANE 7.30 101 415790 8.90 ug/L 100 10) Isopropyl Alcohol 7.90 45 16066 18.06 ug/L 99 11) l,l,2-Trichloro-l,2,2-trif 8.21 101 5429 0.26 ug/L 88 12) ACETONE 8.28 43 225531 41.61 ug/L 95 13) 1,1-DICHLOROETHENE 8.63 61 438072 7.82 ug/L 99 14) METHYLENE CHLORIDE 9.64 49 443904 8.92 ug/L 95 15) METHYL TERT BUTYL ETHER 9.94 73 571458 11.36 ug/L 98 16) TRANS-1,2-DICHLOROETHENE 10.30 61 474927 8.44 ug/L 99 17) 1,1-DICHLOROETHANE 11.19 63 571628 8.87 ug/L 99 18) 2-BUTANONE (MEK) 12.02 43 256067 37.14 ug/L 100 19) 2,2-DICHLOROPROPANE 12.41 77 417485 8.23 ug/L 96 20) CIS-1,2-DICHLOROETHENE 12.50 96 357488 9.44 ug/L 99 21) CHLOROFORM 12.84 83 676869 9.71 ug/L 100 22) BROMOCHLOROMETHANE 13.21 49 261102 9.02 ug/L 98 23) 1,2-DICHLOROETHANE 14.56 62 499142 10.36 ug/L 99 26) 1,1,1-TRICHLOROETHANE 13.74 97 497257 11.52 ug/L 99 27) 1,1-DICHLOROPROPENE 14.06 75 405738 10.22 ug/L 98 28) CARBON TETRACHLORIDE 14.32 117 422660 11.38 ug/L 98 29) BENZENE 14.66 78 1059878 10.72 ug/L 97 30) TRICHLOROETHENE 15.94 95 334218 10.82 ug/L 96 31) 1,2-DICHLOROPROPANE 16.29 63 279343 10.82 ug/L 97 32) DIBROMOMETHANE 16.96 174 176861 12.09 ug/L 93 33) BROMODICHLOROMETHANE 16.81 83 462815 11.84 ug/L 99 34) 2-CHLOROETHYL VINYL ETHER 17.30 63 112768 10.95 ug/L 95 35) METHYL ISO-BUTYL KETONE 17.37 58 213602 48.47 ug/L 97 36) CIS-1,3-DICHLOROPROPENE 17.91 75 373467 9.98 ug/L 99 37) TOLUENE 18.66 91 1011501 9.55 ug/L 98 38) TRANS-1,3-DICHLOROPROPENE 18.93 75 280852 10.17 ug/L 96 39) 1,1,2-TRICHLOROETHANE 19.32 97 187259 10.71 ug/L 95 40) TETRACHLOROETHENE 20.11 166 310432 9.90 ug/L 99 41) 1,3-DICHLOROPROPANE 19.85 76 333748 10.36 ug/L 99 42) DIBROMOCHLOROMETHANE 20.55 129 242010 10.72 ug/L 96 43) 1,2-DIBROMOETHANE 21.01 107 185601 10.41 ug/L 99 44) CHLOROBENZENE 21.88 112 693700 9.72 ug/L 97 45) 1,1,1,2-TETRACHLOROETHANE 21.93 131 268208 10.65 ug/L 98 46) 2-HEXANONE 19.22 43 350615 42.98 ug/L 95 (#) = qualifier out of range (m) = manual integration 0321C10A.D HP031802.M Fri Mar 22 09:11:51 2002 Page 1

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