VOC analysis results, sample AE12738, June 4 2002

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Data File C:\HPCHEM\l\DATA\02june04\0604C10A.D Vial: 11 Acq On 4 Jun 2002 8:32 pm Operator: 201-wb Sample cal 10 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: GAS6.P Quant Time: Jun 4 21:10 2002 Quant Results File: HP052902.RES Quant Method C:\HPCHEM\1\METHODS\HP052902.M (RTE Integrator) Title VOCs BY EPA METHOD 524 Last Update Fri May 31 14:34:13 2002 Response via Initial Calibration DataAcq Meth HP052902

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-DIFLUOROBENZENE 15.09 114 1669373 5.00 ug/L -0.02 24) CHLOROBENZENE-D5 21.75 117 1583646 5.00 ug/L 0.00 52) 1,4-DICHLOROBENZENE-D4 26.93 152 776450 5.00 ug/L 0.00 System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 14.32 65 742717 4.92 ug/L -0.02 Spiked Amount 5.000 Recovery = 98.40% 3) 4-BROMOFLUOROBENZENE 24.34 174 610293 4.59 ug/L 0.00 Spiked Amount 5.000 Recovery = 91.80% 25) TOLUENE-D8 18.45 98 2068059 5.18 ug/L -0.02 Spiked Amount 5.000 Recovery 103.60% . Target Compounds Qvalue 4) DICHLORODIFLUOROMETHANE 4.85 85 477924 8.02 ug/L 99 5) CHLOROMETHANE 5.35 50 679341 7.34 ug/L 98 6) VINYL CHLORIDE 5.59 62 403414 8.42 ug/L 97 7) BROMOMETHANE 6.56 94 272532 10.43 ug/L 100 8) CHLOROETHANE 6.71 64 393913 9.18 ug/L 97 9) TRICHLOROFLUOROMETHANE 7.27 101 651942 9.18 ug/L 99 10) Isopropyl Alcohol 7.87 45 280678 181.44 ug/L 96 11) 1,1,2-Trichloro-l,2,2-trif 8.17 101 514838 9.45 ug/L 94 12) ACETONE 8.24 43 404312 23.21 ug/L 99 13) 1,1-DICHLOROETHENE 8.60 61 1019351 8.49 ug/L 99 14) METHYLENE CHLORIDE 9.60 49 949275 8.51 ug/L 94 15) METHYL TERT BUTYL ETHER 9.91 73 743422 8.61 ug/L 98 16) TRANS-1,2-DICHLOROETHENE 10.27 61 1055123 8.55 ug/L 96 17) 1,1-DICHLOROETHANE 11.17 63 1218817 8.82 ug/L 99 18) 2-BUTANONE (MEK) • 11.99 43 421158 32.31 ug/L 97 19) 2,2-DICHLOROPROPANE 12.38 77 792742 7.69 ug/L 100 20) CIS-1,2-DICHLOROETHENE 12.47 96 704504 9.74 ug/L 91 21) CHLOROFORM 12.81 83 1319210 9.29 ug/L 99 22) BROMOCHLOROMETHANE 13.18 49 525528 8.63 ug/L 96 23) 1,2-DICHLOROETHANE 14.53 62 912507 9.22 ug/L 98 26) 1,1,1-TRICHLOROETHANE 13.71 97 982556 9.59 ug/L 99 27) 1,1-DICHLOROPROPENE 14.03 75 9'07394 9.39 ug/L 97 28) CARBON TETRACHLORIDE 14.29 117 824450 9.64 ug/L 99 29) BENZENE 14.63 78 2342660 9.89 ug/L 99 30) TRICHLOROETHENE 15.91 95 689349 9.72 ug/L 97 31) 1,2-DICHLOROPROPANE 16.27 63 600005 9.63 ug/L 99 32) DIBROMOMETHANE 16.93 174 295436 10.30 ug/L 96 33) BROMODICHLOROMETHANE 16.78 83 871181 9.77 ug/L 98 34) 2-CHLOROETHYL VINYL ETHER 17.25 63 171634 9.32 ug/L 98 35) METHYL ISO-BUTYL KETONE 17.34 58 363627 41.24 ug/L 99 36) CIS-1,3-DICHLOROPROPENE 17.87 75 787566 9.63 ug/L 99 3 7) TOLUENE 18.63 91 2443732 9.88 ug/L 98 38) TRANS-1,3-DICHLOROPROPENE 18.91 75 560165 9.56 ug/L 99 39) 1,1,2-TRICHLOROETHANE 19.30 97 378014 10.38 ug/L 98 4 0) TETRACHLOROETHENE 20.08 166 650079 9.52 ug/L 98 41) 1,3-DICHLOROPROPANE 19.83 76 719678 10.10 ug/L 99 42) DIBROMOCHLOROMETHANE 20.51 129 457735 10.32 ug/L 96 43) 1,2-DIBROMOETHANE 20.97 107 361209 10.01 ug/L • 96 44) CHLOROBENZENE 21.84 112 1581620 10.10 ug/L 97 45) 1,1,1,2-TETRACHLOROETHANE 21.89 131 536224 10.27 ug/L 97 46) 2-HEXANONE 19.18 43 666985 38.79 ug/L 98

(#) = qualifier out of range (m) = manual integration 0604C10A.D HP052902.M Tue Jun 04 21:10:39 2002 Page 1

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