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GCMS analysis results for sample AD25037, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD25037 conducted on November 19, 2001, identifying unknown compounds.

NYC-WTC_000069204–000069214

Folder label: “GCMS Scan X 10/19/01 An 11/8/01

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Scanned page image, NYC-WTC_000069213
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NYC 9/11 Public Portal Document

1 Library Search Compound Report Data File ; C:\HPCHEM\1\DATA\NOV0801\25037.D Vial: 11 Acq On : 9 Nov 2001 12:22 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1,4-Dichlorobenzene-d4 Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 11.57 0.54 ug/1 119031 1,4-Dichlorobenzene-d4 11.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,4-Dichlorobe?fzene-d4 150 C6C12D4 003855-82-1 53 2 Benzene-1,2,3<4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 25 3 Benzenamine< N-methyl-4-nitro- 152 C7H8N2O2i 000100-15-2 14 4 Benzaldehyde, 2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 10 Ahundance / Scan 711 (11.569 min); 25037.D {-) m/z 149.90 100.00% 1$0

5000 115

52 78 40 11 20 11.40 11.60 11.80

7T/z-> 20 .............I' 30 40 50 60 87 Ji 70 80 90 100 110 120 130 140 150 160 ■ m7z“l^lT9T~“69783% Sundance #9593; 1,4-Dichlorobenzene-d4 1!i0

5000 115 78 11.20 11.40 11.60 11.80 52 m/z 114.90 39.72%

Tife-> 20 30 35 40 50 60 70 JU 80 90 100 110 120 130 140 150 160 4^ Wsundance #9592; Benzene-1.2,3,4-d4-, 5,6-dichloro- 150 I 115 11 20 11.40 11.60 11.80 5000 52 78 m/z 77.95 19?^^

35 87 ( ' I ' ' ' ' I ' I ' I ' ' ' ' I ‘ I'''' I 114^ Tt/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #10120; Benzenamine, N-methyl-4-nitro- 1$2 1120 11.40 11.60 11.80 m/z 52.00 16.18% 77 122 110 5000 65 30 94

■nZz-> 20 , , , , I.... . 30 40 , .. ., 1 , I 50 60 70 J... J..,.lll.l„ 80 90 ' ' I ' ' ‘ ' I ' ' ' ' I 100 110 120 130 140 150 11.20 11.40 11.60 11.80

25037.D NP103001.M Mon Nov 19 12:15:32 2001 Page 2

NYC-WTC_000069213

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NYC-WTC_000069213Source: NYC Law Department, mirrored locally

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