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GCMS analysis results for sample AD24873, Nov 2001

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Laboratory report documenting GCMS analysis of sample AD24873 identifying unknown compounds on November 19, 2001.

NYC-WTC_000068942–000068953

Folder label: “GCMS Scan X 10/17/01 An 11/6/01

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Scanned page image, NYC-WTC_000068952
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0601\24873.D Vial: 2 Acq On : 6 Nov 2001 1:46 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1,4-Dichlorobenzene-d4 Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.57 0.54 ug/1 109688 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Taritative ID MW MolForm CAS# Qual 1 1,4-Dichi probenzene-d4 150 C6C12D4 003855-82-1 90 2 Benzene ,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 28 3 Benzend;imine, 2-methyl-4-nitro- 152 C7H8N202I 000099-52-5 16 4 Benzenamine, 2-methyl-5-nitro- 152 C7H8N2O2I 000099-55-8 12 Mxindance Scan 711 (11.572 min): 24873.D (-) m/z 149.90 100.00% 1ii0

5000 115 78 52 T 38 45 Tjra_J 87 IIJO 11.40 11.60 11,80 12.00 '' I' .1 I'l l i l l /■. I . I .1 It] . ' I •'" I'''' I' ....... . m/z 151.90 63.41% nZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Mxjndance #9593:1,4-DichlorobenzBne^ 1!i0

5000 115 .......... 78 11.20 11.40 11.60 11.80 12.00 52 m/z 114.90 . 37.88% 35 TiZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 ^bunciance #9592: Benzenfr-1,2,3,4-{j4-, 5,6<lichloro- 1$0

115 11.20 11.40 11.60 11.80 12.00 5000 52 78 m/z 78705 23.62%

30 35 I 40 50 Tp-n-rp- 60 70 U... u... 80 90 100 110 120 130 140 150 160 Abundance #10129: Benzenamine, 2-methyl-4-nitro- ........ ............ 77 106 1!2 11.20 11.40 11,60 11.80 12.00 m/z 75.90 . 13.89%

5000- 51 94

Tlfe-> ‘ I ’ ’ ’ ' 1 ‘ 30 40 ‘ 1 ' 50 60 70 1 80 90 T 100 110 I ‘ ‘ 130 ’ I • ’'' I 140 150 160 i'i ■»' nl4b' 'iteo 'i'i'm ‘i25oo

24873.D NP103001.M Fri Nov 16 11:52:31 2001 Page 3

NYC-WTC_000068952

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NYC-WTC_000068952Source: NYC Law Department, mirrored locally

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