GCMS calibration table for TCLP analysis, Nov 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0101\LBA.D Vial: 8 Acq On : 1 Nov 2001 9:51 pm Operator: 209 GALOS Sample : 10/11 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 l,4-Dichlorobenzene-d4 Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.58 0.54 ug/1 78328 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tent^ive ID MW MolForm CAS# Qual 1 l,4-Dichlorob^zene-d4 150 C6C12D4 003855-82-1 86 2 2-Adamantanone 150 C1OH140 000700-58-3 25 3 Benzene-l,/,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 16 4 Vanillin / 152 C8H8O3 000121-33-5 9 Abundance Scan 712 (11.581 min): LBA.D (-) m/z 149.90 100.00% 1!i0

5000 115 52 78 40 I 11 87 1120 11.40 11.60 11.80 12.00 I m/z 151.90 . 62.35% -- I ' ' ' ' I tt/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 liO

5000 115 78 11.20 11.40 11.60 11.80 12.00 52 m/z 114.90 . 35.63% 35 4^ nZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9842:2-Adamantanone 1!i0

79 11.20 11.40 11.60 11,80 12.00 5000 m/z 77.95 , 15.74%

93 104 17 11 132 ' I ‘ ■ T nZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichioro- .................... / , ........... 1!i0 11.^20 '11'40' 'I'tCT 11’80 '1'200 m/z 52.00 14.30% 115 5000 52 78

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inZz-> ' ' 1 ' ' ' ‘ I ‘ 30 40 ' I 50 ‘ ' I ' ' ' ’ 1 ’ ' 60 70 r' ’'' I''' H 80 90 1(X) ‘’ 1' * 110 120 130 140 150 ku. 160 i'i.'^' ii.4o' 'ii!a '11.80' '12I00

LBA.D NP103001.M Wed Nov 07 14:58:15 2001 Page 3

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