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GCMS calibration table for TCLP analysis, Oct 31 2001

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Calibration data sheet listing surrogate compounds and retention times for GC/MS instrument used in TCLP testing on October 31, 2001.

NYC-WTC_000067940–000067949

Folder label: “GCMS Scan X 10/9/01 An 10/31/01

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NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed) Data File : C:\HPCHEM\l\data\oct3001\LBA.D Vial; 21 Acq On : 31 Oct 2001 11:26 am Operator: 209 GALOS Sample ; lab blk 10/9 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time; Oct 31 12:15 2001 Quant Results File; NP101901.RES Quant Method ; C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title ; 209 625/TCLP calibration table Last Update ; Tue Oct 23 10:12:13 2001 Response via ; Initial Calibration DataAcq Meth ; NP101901

Compound R.T. Qlon Response Cone Unit Qvalue 23) 2-Nitrophenol 0.00 139 0 N.D. 24) 2,4-Dimethylphenol 0.00 107 0 N.D. 25) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 26) 2,4-Dichlorophenol 0.00 162 0 N.D. 27) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 28) Naphthalene 0.00 128 0 N.D. 29) Hexachlorobutadiene 0.00 225 0 N.D. 30) 4-Chloro-3-methylphenol 0.00 107 0 N.D. 34) Hexachlorocyclopentadiene 0.00 237 0 N.D. 35) 2,4,6-Trichlorophenol 0.00 196 0 N.D. 36) 2,4,5-Trichlorophenol 0.00 196 0 N.D. 37) 2-Chloronaphthalene 0.00 162 0 N.D. 3 8) Dimethylphthalate 0.00 163 0 N.D. 39) 2,6-Dinitrotoluene 20.60 165 228683 4.88 ug/1 # 44 4 0) Acenaphthylene 0.00 152 0 N.D. 41) Acenaphthene 0.00 153 0 N.D. 42) 2,4-Dinitrophenol 0.00 184 0 N.D. 43) 4-Nitrophenol 21.04 65 1228 N.D. 44) 2,4-Dinitrotoluene 21.28 165 180 N.D. 45) Diethylphthalate 0.00 149 0 N.D. 46) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 47) Fluorene 0.00 166 0 N.D. 48) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 50) 4,6-Dinitro-2-methylphenol 0.00 198 0 N.D. 51) N-Nitrosodiphenylamine 0.00 168 0 N.D. 52) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 53) Hexachlorobenzene 0.00 284 0 N.D. 54) Pentachlorophenol 0.00 266 0 N.D. 55) Phenanthrene 25.03 178 988 N.D. 5 6) Anthracene 25.03 178 988 N.D. 57) Di-n-butylphthalate 27.03 149 3270 N.D. 5 8) Fluoranthene 0.00 202 0 N.D. 60) 3,3'-Dichlorobenzidine 0.00 252 0 N.D. 61) Benzidine 29.20 184 7493 N.D. 63) Pyrene 0.00 202 0 N.D. 64) Butylbenzylphthalate 0.00 149 0 N.D. 65) Benz o(a)anthracene 33.06 228 3640 N.D. 66) Bis(2-ethylhexyl)phthalate 33.32 149 904 N.D. 67) Chrysene 33.06 228 3640 N.D. 69) Di-n-Octylphthalate 35.07 149 606 N.D. 70) Benzo(b)fluoranthene 0.00 252 0 N.D. (#) = qualifier out of range (m) = manual integration LBA.D NP101901.M Wed Oct 31 12:15:43 2001 Page 2

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