NYC-WTC_000067623
DEP lab report for GCMS analysis of sample AD23914 conducted on October 25, 2001, noting unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Document / 10 pages
GCMS calibration table for TCLP analysis, Oct 31 2001
Machine-extracted title · confidence 95%Calibration data sheet listing surrogate compounds and retention times for GC/MS instrument used in TCLP testing on October 31, 2001.
NYC-WTC_000067940–000067949Folder label: “GCMS Scan X 10/9/01 An 10/31/01”
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NYC 9/11 Public Portal Document
Quantitation Report (Not Reviewed) Data File : C:\HPCHEM\l\data\oct3001\LBA.D Vial: 21 Acq On : 31 Oct 2001 11:26 am Operator: 209 GALOS Sample : lab blk 10/9 Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Oct 31 12:15 2001 Quant Results File: NP101901.RES Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Oct 23 10:12:13 2001 Response via : Initial Calibration DataAcq Meth : NP101901
Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.72 152 944964 20.00 ug/1 -0.04 19) Naphthalene-d8 15.32 136 3719166 20.00 ug/1 -0.04 31) Acenaphthene-dlO 20.60 164 1785657 20.00 ug/1 -0.03 49) Phenanthrene-dlO 25.03 188 2602584 20.00 ug/1 -0.03 59) Chrysene-dl2 33.06 240 1502043 20.00 ug/1 -0.04 68) Perylene-dl2 37.16 264 995544 20.00 ug/1 -0.03 System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 5) Phenol-d5 0.00 99 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 6) 2-Chlorophenol-d4 11.71 132 534 0.01 ug/1 0.44 Spiked Amount 75.000 Recovery = 0.01% 7) 1,2-Dichlorobenzene-d4 12.23 152 10545 0.16 ug/1 -0.04 Spiked Amount 50.000 Recovery = 0.32% 20) Nitrobenzene-d5 0.00 82 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% 32) 2-Fluorobiphenyl 18.75 172 3681 0.02 ug/1 0.10 Spiked Amount 50.000 Recovery = 0.04% 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 62) Terphenyl-dl4 0.00 244 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitroso-dimethyl amine 5.27 74 368 N.D. 8) Phenol 0.00 94 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 10) 2-Chlorophenol 0.00 128 0 N.D. 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146 0 N.D. 13) 1,2-Dichlorobenzene 0.00 146 0 N.D. 14) 2-Methylphenol 0.00 108 0 N.D. 15) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 16) 3&4-Methylphenol 0.00 108 0 N.D. 17) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 18) Hexachloroethane 0.00 117 0 N.D. 21) Nitrobenzene 0.00 77 0 N.D. 22) Isophorone 0.00 82 0 N.D. (#) = qualifier out of range (m) = manual integration LBA.D NP101901.M Wed Oct 31 12:15:38 2001 Page 1
NYC-WTC_000067940
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