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← Document results/DEP Box 60/GCMS Scan X 10/2/01 An 10/17/01
Document / 11 pages

GCMS calibration table, Oct 17 2001

Machine-extracted title · confidence 90%

Laboratory report detailing GCMS analysis of sample AD22558 conducted on October 1, 2001.

NYC-WTC_000067428–000067438

Folder label: “GCMS Scan X 10/2/01 An 10/17/01”

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NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed) Data File : C:\HPCHEM\1\DATA\OCT1701\LB.D Vial: 2 Acq On : 17 Oct 2001 2:09 pm Operator: 209 GALOS Sample : lab blk 10/2 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Oct 17 14:59 2001 Quant Results File: NP091101.RES Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Last Update : Fri Oct 12 09:04:47 2001 Response via : Initial Calibration DataAcq Meth : NP091101

Compound R.T. Qlon Response Cone Unit Qvalue 23) 2-Nitrophenol 0.00 139 0 N.D. 24) 2,4-Dimethylphenol 0.00 107 0 N.D. 25) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 26) 2,4-Dichlorophenol 0.00 162 0 N.D. 27) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 2 8) Naphthalene 0.00 128 0 N.D. 29) Hexachlorobutadiene 0.00 225 0 N.D. 30) 4-Chloro-3-methylphenol 0.00 107 0 N.D. 34) Hexachlorocyclopentadiene 0.00 237 0 N.D. 35) 2,4,6-Trichlorophenol 0.00 196 0 N.D. 36) 2,4,5-Trichlorophenol 0.00 196 0 N.D. 37) 2-Chloronaphthalene 0.00 162 0 N.D. 3 8) Dimethylphthalate 0.00 163 0 N.D. 39) 2,6-Dinitrotoluene 0.00 165 0 N.D. 4 0) Acenaphthylene 0.00 152 0 N.D. 41) Acenaphthene 0.00 153 0 N.D. 42) 2,4-Dinitrophenol 0.00 184 0 N.D. 43) 4-Nitrophenol 0.00 65 0 N.D. 44) 2,4-Dinitrotoluene 0.00 165 0 N.D. 45) Diethylphthalate 0.00 149 0 N.D. 46) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 47) Fluorene 0.00 166 0 N.D. 48) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 50) 4,6-Dinitro-2-methylphenol 0.00 198 0 N.D. 51) N-Nitrosodiphenylamine 0.00 168 0 N.D. 52) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 53) Hexachlorobenzene 0.00 284 0 N.D. 54) Pentachlorophenol 0.00 266 0 N.D. 5 5) Phenanthrene 0.00 178 0 N.D. 56) Anthracene 0.00 178 0 N.D. 57) Di-n-butylphthalate 27.08 149 816 N.D. 5 8) Fluoranthene 0.00 202 0 N.D. 60) 3,3'-Dichlorobenzidine 0.00 252 0 N.D. 61) Benzidine 29.27 184 5114 N.D. 63) Pyrene 0.00 202 0 N.D. 64) Butylbenzylphthalate 0.00 149 0 N.D. 65) Benz o(a)anthracene 33.13 228 1875 N.D. 66) Bis(2-ethylhexyl)phthalate 33.39 149 1036 N.D. 67) Chrysene 33.13 228 1875 N.D. 69) Di-n-Octylphthalate 0.00 149 0 N.D. 70) Benzo(b)fluoranthene 0.00 252 0 N.D.

(#) = qualifier out of range (m) = manual integration LB.D NP101901.M Tue Oct 23 14:45:53 2001 Page 2

NYC-WTC_000067429

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NYC-WTC_000067429Source: NYC Law Department, mirrored locally

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GCMS sample extraction log table, Nov 2001 · Box DEP Box 60

NYC-WTC_000068400

Multi-page laboratory log table recording sample extraction details including volumes and drip rates for GCMS analysis in November 2001.

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