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← Document results/DEP Box 60/GCMS Scan X 10/2/01 An 10/17/01
Document / 11 pages

GCMS calibration table, Oct 17 2001

Machine-extracted title · confidence 90%

Laboratory report detailing GCMS analysis of sample AD22558 conducted on October 1, 2001.

NYC-WTC_000067428–000067438

Folder label: “GCMS Scan X 10/2/01 An 10/17/01”

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NYC 9/11 Public Portal Document

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Quantitation Report (Not Reviewed) Data File : C;\HPCHEM\1\DATA\OCT1701\LB.D Vial: 2 Acq On : 17 Oct 2001 2:09 pm Operator: 209 GALOS Sample : lab blk 10/2 z Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Oct 17 14:59 2001..^-^.7 ' Quant Results File: NP091101.RES Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Last Update : Fri Oct 12 09:04:47 2001 Response via : Initial Calibration DataAcq Meth : NP091101

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.77 152 406020 20.00 ug/1 -0.14 19) Naphthalene-d8 15.38 136 1597136 20.00 ug/1 -0.15 31) Acenaphthene-dlO 20.65 164 764790 20.00 ug/1 -0.16 49) Phenanthrene-dlO 25.09 188 1098522 20.00 ug/1 -0.15 59) Chrysene-dl2 33.12 240 823340 20.00 ug/1 -0.16 68) Perylene-dl2 37.24 264 616089 20.00 ug/1 -0.18

System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 5) Phenol-d5 0.00 99 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 6) 2-Chlorophenol-d4 0.00 132 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 7) 1,2-Dichlorobenzene-d4 12.28 152 4129 0.21 ug/1 -0.15 Spiked Amount 50.000 Recovery = 0.42% 20) Nitrobenzene-d5 0.00 82 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% 32) 2-Fluorobiphenyl 18.80 172 1523 0.03 ug/1 -0.01 Spiked Amount 50.000 Recovery = 0.06% 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 62) Terphenyl-dl4 0.00 244 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitroso-dimethyl amine 0.00 74 0 N.D. 8) Phenol 0.00 94 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 10) 2-Chlorophenol 0.00 128 0 N.D. 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146 0 N.D. 13) 1,2-Dichlorobenzene 0.00 146 0 N.D. 14) 2-Methylphenol 0.00 108 0 N.D. 15) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 16) 3&4-Methylphenol 0.00 108 0 N.D. 17) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 18) Hexachloroethane 0.00 117 0 N.D. 21) Nitrobenzene 0.00 77 0 N.D. 22) Isophorone 0.00 82 0 N.D.

(#) = qualifier out of range (m) = manual integration LB.D NP101901.M Tue Oct 23 14:45:47 2001 Page 1

NYC-WTC_000067428

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NYC-WTC_000067428Source: NYC Law Department, mirrored locally

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GCMS sample extraction log table, Nov 2001 · Box DEP Box 60

NYC-WTC_000068400

Multi-page laboratory log table recording sample extraction details including volumes and drip rates for GCMS analysis in November 2001.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995

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