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GC/MS TCLP calibration table analysis, October 2001

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GC/MS analysis report with TCLP calibration table data from October 16, 2001.

NYC-WTC_000089030–000089044

Folder label: “GC/MS Scan 9/28/01

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NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed) Data File : C:\HPCHEM\1\DATA\OCT1501\LB.D Vial: 3 Acq On : 15 Oct 2001 1:28 pm Operator: 209 GALOS Sample : lab blk 9/28 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Oct 16 8:08 2001 Quant Results File: NP091101'.RES Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Last Update : Fri Oct 12 09:04:47 2001 Response via : Initial Calibration DataAcq Meth : NP091101

Compound R.T. Qlon Response Cone Unit Qvalue 23) 2-Nitrophenol 0.00 139 0 N.D. 24) 2,4-Dimethylphenol 0.00 107 0 N.D. 25) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 26) 2,4-Dichlorophenol 0.00 162 0 N.D. 27) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 28) Naphthalene 0.00 128 0 N.D. 29) Hexachlorobutadiene 0.00 225 0 N.D. 30) 4-Chloro-3-methylphenol 0.00 107 0 N.D. 34) Hexachlorocyclopentadiene 0.00 237 0 N.D. 35) 2,4,6-Trichlorophenol 0.00 196 0 N.D. 36) 2,4,5-Trichlorophenol 0.00 196 0 N.D. 37) 2-Chloronaphthalene 0.00 162 0 N.D. 38) Dimethylphthalate 0.00 163 0 N.D. 39) 2,6-Dinitrotoluene 20.66 165 99254 7.71 ug/1 # 46 40) Acenaphthylene 0.00 152 0 N.D. 41) Acenaphthene 0.00 153 0 N.D. 42) 2,4-Dinitrophenol 0.00 184 0 N.D. 43) 4-Nitrophenol 0.00 65 0 N.D. 44) 2,4-Dinitrotoluene 0.00 165 0 N.D. 45) Diethylphthalate 0.00 149 0 N.D. 46) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 47) Fluorene 0.00 166 0 .N.D. 48) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 50) 4,6-Dinitro-2-methylphenol 0.00 198 0- N.D. 5T-)—N-Nitrosodiphenylamine---- OvOO—1’68 --- ^0- -n;d;— 52) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 53) Hexachlorobenzene 0.00 284 0 N.D. 54) Pentachlorophenol 0.00 266 0 . N.D. 5 5) Phenanthrene 25.07 178 294 N.D. 56) Anthracene 25.07 178 294 N.D. 57-)—Di-n-butylphthalate - -—--- -27-.-09 -149 ~2-3-4-0-‘ -N-tDt-— 5 8) Fluoranthene 0.00 202 0- N.D. 60) 3,3'-Dichlorobenzidine O-. OO- -252 - -0 N.D. ■±r-;r6T-)-^Benzidine^^^—Y OTOO“18L4t^ — rNVDTZr ' ^6 3')~ Pyrene 0.00 202 0 N.D. 64) Butylbenzylphthalate 0.00 149 0 N.D. 65) Benzo.(a)_anthracene _ 33.13 228 17.8:0 . N.D. ■6'6-)—Bi-s-(-2—ethylh’e*XYl)-phtha-late^33~3'8 ■1"4'9“ “l'9'0'9r 'NTD7~ 67) Chrysene 33.13 228 1780 N.D. 69) Di-n-Octylphthalate 0.00 149 0 N.D. 70) Benzo(b)fluoranthene 0.00 252 0. N.D. (#) = qualifier out of range (m) = manual integration LB.D NP091101.M Tue Oct 16 08:25:34 2001 Page 2

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