GC/MS analysis report with TCLP calibration table data from October 16, 2001.
NYC-WTC_000089030–000089044Folder label: “GC/MS Scan 9/28/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (Not Reviewed) Data File : C:\HPCHEM\1\DATA\OCT1501\LB.D / Vial: 3 Acq On : 15 Oct 2001 1:28 pm Operator: 209 GALOS Sample : lab blk 9/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Oct 16 8:08 2001 ^Quant Results File: NP091101.RES
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Last Update : Fri Oct 12 09:04:47 2001 Response via : Initial Calibration DataAcq Meth : NP091101
Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-DichIorobenzene-d4 11.76 152 424582' . 20.00 ug/1 -0.14 19) Naphthalene-d8 15.38 136 1655205. 20.00 ug/1 -0.14 31) Acenaphthene-dlO 20.66 164 787287 20.00 ug/1 -0.15 49) Phenanthrene-dlO 25.08 188 1147596 20.00 ug/1 -0.15 59) Chrysene-dl2 33.13 240 784418 20.00 ug/1 -0.15 68) Perylene-dl2 37.23 264 566229 20^00 ug/1 ■-0.19
System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ug/1 Spiked Amount 75.000 Recoveisy = 0.00% 5) Phenol-d5 . 0.00 99 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 6) 2-Chlorophenol-d4 0.00 132 0 0.00 ug/1 Spiked Amount 75.000 Recovery 0.00% 7) 1,2-Dichlorobenzene-d4 12.29 152 4326 0.21 ug/1 -0.14 Spiked Amount 50.000 Recovery = 0.42% 20) Nitrobenzene-d5 0.00 82 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00%' 32) 2-Fluorobiphenyl 18.80 172 1643 0.03 ug/1 0.00 Spiked Amount 50.000 Reedvery = 0.06% 33) 2,4,6-Tribromophenol 0.00 330 0 - 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 62) Terphenyl-dl4 0.00 244 . 0 “ 6.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% Target Compounds- Qvalue 2) Pyridine 0.00 79 0 . N.D. 3) N-nitroso-dimethyl amine 0.00 74 0. N.D. 8) Phenol 0.00 94 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 N.D. —10)—2 - Chlorophenol------- ——----- 0.00—1-28— — -0-^ —N^D^-- 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. -12 )_1,4-Dichlorobenzene — 0.00 - 146- - 0 -N . D .- - “l-3r)=sT*r2-Dichl-orobenzeneT-^r^^-5-- -—---'OrO 0s=sar4 6“- =— -r4‘)^2-Mgthylph^’hdl------------ ------OTO'O—1’0’8----- N.D. 15) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 16 )_3 &4 -Methylphenol. 0.00. 108_ 0 . _N.D.._ 17 j-^N - Ni t r os o~di-n-p r opy l-am±ne“'~:0T0:0 -70- -N-DT~ 18) Hexachloroethane 0.00 117 0 N.D. 21) Nitrobenzene 0.00 77 0 . N.D. 22) Isophorone 0.00 82 0 N.D. (#) = qualifier out of range (m) = manual integration LB.D NP091101.M Tue Oct 16 08:25:29 2001 Page 1
NYC-WTC_000089030
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NYC-WTC_000088491
Calibration data table for TCLP analysis using GC/MS standards processed on October 18, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088700
Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088184
Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089278
GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000086624
Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000086788
Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000087496
Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067739
Calibration data sheet listing surrogate compounds and retention times for GC/MS instrument used in TCLP testing on October 25, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068559
Calibration data table for GC/MS instrument used in TCLP analysis, generated on November 5, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067428
Laboratory report detailing GCMS analysis of sample AD22558 conducted on October 1, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068400
Multi-page laboratory log table recording sample extraction details including volumes and drip rates for GCMS analysis in November 2001.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067979
Calibration data table for GCMS TCLP analysis listing surrogate compounds and response factors from November 2, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.993
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